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GCMS analysis report sample AE09682, May 23, 2002

Machine-extracted title · confidence 95%

GCMS laboratory report for sample AE09682 detecting unknown compounds and 2,4-DDD on May 23, 2002.

NYC-WTC_000013258–000013276

Folder label: “GCMS X 5/21/02 A 5/21/02

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NYC 9/11 Public Portal Document Llbrary searcn compound keport Data File : C:\MSDCHEM\l\DATA\052102\9682.D Vial: 18 Acq On : 22 May 2002 3:11 am Operator: Mclean Sample : re-extract Inst : Instrumen Mise : Multiplr: 1.00 MS Integration Params: LSCINT.e

Quant Method : C:\MSDCHEM\1\METHODS\052202.M (Chemstation Integrator) Title : 508 Modified GC/MS scan Library : C:\DATABASE\NIST98.L ****************************************** * * ************************* Peak Number 10 Anthracene-dlO- Concentration Rank 11

R.T. EstConc Area Relative to ISTD R.T.

23.07 0.26 ug/L 274635 Phenanthranene-dl0 22.91

Hit# of 5 Tentative ID MW MolForm CAS# Qual 1 Anthracene-dlO- 188 C14D10 001719-06-8 90 2 Phenanthrene-diO 188 C14D10 001517-22-2 43: 3 Naphthalene, 1,7-dimethoxy- 188 C12H12O2 005309-18-2 40 4 2-Quinolinecarboxaldehyde, 8-hyd... 188 C10H8N2O2 005603-22-5 38 Abundance Scan 3402 (23.068 min): 9682.D (-3396) (-) m/z 188.10 100.00% 188

5000

80 94 160 22.80 23.00 23.20 23.40 miz-> 0 ।.... ।.... ।..., 42 m !‘T । r... ।.... 1..66 J .11I .. ।. 11111111111 10 20 30 40 50 60 70 80 90 100110 120 130 140 150 160 170 180 190 m/z 184.10 17.14% Abundance #79826: Anthracene-d10- 188

5000 ■ r-] • i i i । i > i i 22.80 23.00 23.20 23.40 m/z 94.10 17.09% 80 94 160 17 30 42 52 । | J 108118 132 146 ,1, 170179 0- mmhugttpmtmmpm lz-> 10 20 30 40 50 60 70 80 90 100110 120 130 140 150 160 170 180 190 Abundance #79827: Phenanthrene-d10 188 ........... .......................................

22.80 23.00 23.20 23.40 5000 m/z 189.20 16.19%

«« 80 94 160 30 42 52 66 । 108 118 132 146 J 1701791, | 0- niz-> 10 20 30 40 50 60 70 80 90 100110120130140150160170180190 Abundance #79804: Naphthalene, 1,7-dimethoxy- 173 188 22.80 23.00 23.20 23.40 m/z 80.00 11.10% 5000 102 115 145

51 63 75 ( 130 158

/z—> 10 20 30 40 50 60 70 80 90 100110120 130140150160170180190 22.80 23.00 23.20 23.40

9682.D 052202.M Wed May 22 11:46:58 2002 Page 12

NYC-WTC_000013274

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NYC-WTC_000013274Source: NYC Law Department, mirrored locally

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