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GCMS analysis results for unknown compounds, June 2002

Machine-extracted title · confidence 90%

Laboratory report documenting GCMS analysis of sample AE12735 with surrogate recovery data and identification of unknown compounds.

NYC-WTC_000015200–000015223

Folder label: “GCMS X 6/3/02 A 6/7/02

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NYC 9/11 Public Portal Document ulbrary searcn compound keport

Data File C:\MSDCHEM\1\DATA\060702\12736.D Vial: 12 Acq On 7 Jun 2002 5:32 pm Operator: Sample Inst : Instrumen Mise Multiplr: 1.00 MS Integration Params: LSCINT.e Quant Method : C:\MSDCHEM\1\METHODS\060302.M (Chemstation Integrator) Title : 508 Modified GC/MS scan Library : C:\DATABASE\NIST98.L ********************************************************************* Peak Number 14 Anthracene-dlO- Concentration Rank 9 R.T. EstConc Area Relative to ISTD R.T. 23.06 0.31 ug/L 331690 Phenant hranene -dl 0 22.91 Hit# of 5 Tentative ID MW MolForm CAS# 1 Anthracene-dlO- 188 C14D10 001719-06-8 83 . oual Q 2 Phenanthrene-diO 188 C14D10 001517-22-2 80 3 Pentacyclo[7.3.1.1.(4,12).0(2,7)... 188 C14H20 1000215-61-8 45 4 Naphthalene, 1,7-dimethoxy- 188 C12H1202 005309-18-2 38 Abundance Scan 3401 (23.062 min): 12736.D (-3395) (-) m/z 188.10 100.00% 188

5000-

80 94 ) 1 158 22.80 23.00 23.20 23.40 42 57 66 . 0-TIPTTPTmTTTTTTHT ■ i11 ■ ■i■1■ ■ i “ " i “ ■ • i ■■" i" —pl ■p-n-r m/z 189.10 19.23% iz-> 10 20 30 40 50 60 70 80 90 100110 120 130 140 150 160 170 180 190 Abundance #79826: Anthracene-d10- 188

5000 - 22.80 23.00 23.20 23.40 m/z 184.10 18.65% 80 94 160 , , 17 30 42 52 66 —108118. 132. 146—1701794. 0 111»111 r« t j 11»111111 ] (I n । r( 111 11 {I 11)) n/z-> 10 20 30 40 50 60 70 80 90 100110 120 130 140 150 160 170 180 190 Abundance #79827: Phenanthrene-d10 168

22.80 23.00 23.20 23.40 5000 m/z 80.10 18.47%

80 94 160 30 42 52 66 I,. 1[ — 0-Yl" ।.p--. (I'... । II.. । rl i 11 108118 132 146 170179—— m/z-> 10 20 30 40 50 60 70 80 90 100110 120 130 140 150 160 170 180 190 Abundance #79715: Pentacyclo[7.3.1.1.(4,12).0(2,7).0(6,11)]tetradeca... 11® 22.80 23.00 23.20 23.40 m/z 94.10 14.36% 5000 79 91 55 67 131 105 117 Oh 11 > > i j ■ > । > p > ■ > 11 — 145 158173..Il ----- n/z—> 10 20 30 40 50 60 70 80 90 100110 120 130 140 150 160 170 180 190 22.80 23.00 23.20 23.40

12736.D 060302.M Mon Jun 10 11:23:36 2002 Page 17

NYC-WTC_000015221

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NYC-WTC_000015221Source: NYC Law Department, mirrored locally

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