GCMS analysis results for sample AD31672, Jan 28 2002

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Data File : C:\MSDCHEM\1\5973N\02JAN17\31672.D Vial: 7 • Acq On : 17 Jan 2002 7:49 pm Operator: Sample : 508 scan Inst : Instrumen Mise : January 17, 2002 Multiplr: 1.00 MS Integration Params: LSCINT.P Quant Method : C:\MSDCHEM\1...\SCAN508.M (RTE Integrator) Title : 508 scan method Library : C:\DATABASE\WILEY7N.L ********************************************************************* Peak Number 7 DECADEUTEROPHENANTHRENE $$ ... Concentration Rank 2 R.T. EstConc Area Relative to ISTD R.T.

22.77 0.33 ug/L 188124 Phenanthrene-dl0 22.63 Hit# of 5 Tentative ID MW MolForm CAS# Qual 1 DECADEUTEROPHENANTHRENE $$ Phena... 188 C14D10 001517-22-2 90 2 Acridine-D9 188 C13D9N 000000-00-0 59 3 Anthracene-D10 188 C14D10 000000-00-0 50 4 Cycloheptanone, 4-phenyl- 188 C13H160 067688-28-2 47 Abundance Scan 1699 (22.771 min): 31672.D (-) m/z 188.15 100.00% 188

5000 94 111 —T—1 , 80 2240 22.60 22.80 23.00 23.20 132 160 /z—> 0- -I 66 — 1i{ p-n-rj- 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 mmmpm 1.. m/z 94.05 25.47%

Abundance #84500: DECADEUTEROPHENANTHRENE $$ Phenanthrene-d10 188

5000 2240 22.60 22.80 '23.00 2320 80 94 m/z 80.00 14.56% — 0- 1 ■ I"‘■i■■■■i“66''i“ 1 ■ miz-> 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 Abundance #85254: Acridine-D9 188

22.40 22.60 22.80 23.00 23.20 5000 m/z 189.20 13.39%

93 158 ——— 0 '‘I‘ ‘I‘ ' I''' ‘ I ‘‘ ‘ I ‘ ' 111 ‘' I ‘ ‘ “ I' ‘ “ I “ “ I' 'I‘ n/z-> 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 Abundance #84498: Anthracena-D10 188 22.40 22.60 2280 23.00 23.20 m/z 184.10 8.82%

5000 80 94 66 160 .1 0 * mnpi 1 ,1 i -i i ■ 11 ■ t ■ । >' m/z—> 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 22.40 22.60 22.80 23.00 23.20

31672.D SCAN508.M Tue Jan 22 08:37:31 2002 Page 9

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