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GCMS blank analysis results for sample AE00327, Jan 2002

Machine-extracted title · confidence 100%

Laboratory report documenting GCMS blank analysis to verify system cleanliness during January 10-11, 2002 testing.

NYC-WTC_000051179–000051191

Folder label: “GCMS X 1/8/02 A 1/10/02

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Scanned page image, NYC-WTC_000051190
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NYC 9/11 Public Portal Document

ulprary Searcn compound Report

Data File : C:\MSDCHEM\1\5973N\02JAN10\0108B.D Vial: 1 Acq On : 10 Jan 2002 12:21 pm Operator: Sample : lab blank ext 1/8 Inst : Instrumen Mise : January 10, 2002 Multiplr: 1.00 MS Integration Params: LSCINT.P

Quant Method : C:\MSDCHEM\1...\SCAN508. M (RTE Integrator) Title : 508 scan method Library : C:\DATABASE\WILEY7N. L Peak Number 7 DECADEUTEROPHENANTHRENE $$ ... Concentration Rank 2 R.T. EstConc Area Relative to ISTD R.T. 22.77 0.33 ug/L 177040 Phenanthrene-dl0 22.65 Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 DECADEUTEROPHENANTHRENE $$ Phena... 188 C14D10 001517-22-2 91 2 Phenanthrene-dlO 188 C14D10 001517-22-2 87 3 Acridine-D9 188 C13D9N 000000-00-0 64 4 Anthracene-dlO- 188 C14D10 001719-06-8 50 Abundance Scan 1699 (22.771 min): 0108B.D (-) m/z 188.10 100.00%

5000

94 . ee 80 158 22.40 22.60 22.80 23.00 23.20

/z—> 0 49 00 । . 1■1»| ■t>| <<I I|I''I|IIr .... I... * 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 m/z 94.10 18.15% Abundance #84500: DECADEUTEROPHENANTHRENE $$ Phenanthrene-d10 188

5000 22.40 22.60 22.80 23.00 23.20 80 94 m/z 189.15 11.76%

/z-> 0 PPPPT 40 50 60 70 80 66 -PPH 158

90 100 110 120 130 140 150 160 170 180 190 —L Abundance #84499: Phenanthrene-d10 188

22.40 22.60 22.80 23.00 23.20 5000 m/z 184.10 11.17%

80 94 160

mtz-> 66 0 TTTTTTPTTT 441Q— 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 Abundance #85254: Acridine-D9 188 22.40 22.60 22.80 23.00 23.20 m/z 158.10 9.95% 5000

158 66 80 —

m/z—> 0 .. I, . . i ■ ■ " i " '' i 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 -------------------------- 22.40 22.60 22.80 23.00 23.20

3108B.D SCAN508.M Fri Jan 11 10:09:15 2002 Page 9

NYC-WTC_000051190

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NYC-WTC_000051190Source: NYC Law Department, mirrored locally

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