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GCMS results for sample AE00464, Jan 24 2002

Machine-extracted title · confidence 100%

Laboratory report showing GCMS analysis of sample AE00464 with surrogate recovery data on January 24, 2002.

NYC-WTC_000051439–000051452

Folder label: “GCMS X 1/8/02 A 1/11/02

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Scanned page image, NYC-WTC_000051451
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OCR status: ok · source: pdftotext

NYC 9/11 Public Portal Document

Library Search Compound Report

Data File : C:\MSDCHEM\1\5973N\02JAN11\00464.D Vial: 6 Acq Cn : 11 Jan 2002 6:15 pm Operator: Sample : 508 scan Inst : Instrumen Mise : January 11, 2002 Multiplr: 1.00 MS Integration Params: LSCINT.P

Quant Method : C:\MSDCHEM\1...\SCAN508 .M (RTE Integrator) Title : 508 scan method Library : C:\DATABASE\WILEY7N.L

Peak Number 7 DECADEUTEROPHENANTHRENE $$ ... Concentration Rank 3

R.T. EstConc Area Relative to ISTD R.T.

22.77 0.26 ug/L 133072 Phenanthrene-dl0 22.63

Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 DECADEUTEROPHENANTHRENE $$ Phena... 188 C14D10 001517-22-2 86 2 Anthracene-dlO- 188 C14D10 001719-06-8 83 3 Anthracene-DlO 188 C14D10 000000-00-0 80 4 Phenanthrene-diO 188 C14D10 001517-22-2 72 Abundance Scan 1699 (22 771 min): 00464.D (-) m/z 188.10 100.00% 188

5000 94 66 80 160 । 22.40 22.60 22.80 23.00 23.20 0 H "I.. ।'I ■ ■ ।. III... il TTT m/z94.05 21.95% m/z—> 60 70 80 90 100 110 120 130 140 150 160 170 180 190 Abundance :#84500: DECADEUTEROPHENANTHRENE $$ Phenanthrene-d10 188

5000 r 22.40 22.60 22.80 23.00 23.20 80 94 m/z 189.15 18.08% 66 158 — 0 I"1'!" — । ■11| > > > ■ i > ■ i ■ ■ ■ ■ i ■ 1 1' i ' ■ ' ' i' ' ' i /z-> 60 70 80 90 100 110 120 130 140 150 160 170 180 190 Abundance #84502: Anthracene-d10- 188

22.40 22.60 22.80 23.00 23.20 5000 m/z 184.10 14.25%

66 80 94 160 — ..................... 0 H m/z-> 60 70 80 90 100 110 120 130 140 150 160 170 180 190 Abundance #84498: Anthracene-D10 188 22.40 22.60 22.80 23.00 23.20 m/z 80-05 12.29%

5000 80 94 66 160 —— - 0 111 /z-> 60 70 80 90 100 110 120 130 140 150 160 170 180 190 22.40 22.60 22.80 23.00 23.20

00464.D SCAN508.M Mon Jan 14 10:47:01 2002 Page 9

NYC-WTC_000051451

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NYC-WTC_000051451Source: NYC Law Department, mirrored locally

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