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GCMS results for sample AE00462, Jan 24 2002

Machine-extracted title · confidence 100%

Laboratory report showing GCMS analysis of sample AE00462 with surrogate recovery data on January 24, 2002.

NYC-WTC_000051408–000051421

Folder label: “GCMS X 1/8/02 A 1/11/02

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Scanned page image, NYC-WTC_000051420
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NYC 9/11 Public Portal Document

Library Search Compound Report Data File : C:\MSDCHEM\1\5973N\02JAN11\00462.D Vial: 4 Acq On : 11 Jan 2002 4:36 pm Operator: Sample : 508 scan Inst : Instrumen Mise : January 11, 2002 Multiplr: 1.00 MS Integration Params: LSCINT.P Quant Method : C:\MSDCHEM\l-..\SCAN508.M (RTE Integrator) Title : 508 scan method Library : C:\DATABASE\WILEY7N.L Peak Number 7 DECADEUTEROPHENANTHRENE $$ ... Concentration Rank 3 R.T. EstConc Area Relative to ISTD R.T. 22.77 0.31 ug/L 188064 Phenanthrene-dl0 22.65 Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 DECADEUTEROPHENANTHRENE $$ Phena... 188 C14D10 001517-22-2 91 2 Phenanthrene-dlO 188 C14D10 001517-22-2 72 3 Anthracene-dlO- 188 C14D10 001719-06-8 72 4 Cycloheptanone, 4-phenyl-188 C13H16O 067688-28-2 47 Abundance Scan 1699 (22.771 min): 00462.D (-) m/z 188.10 100.00% 18 8

5000

80 94 66 160 . 22.40 22.60 22.80 23.00 23.20 0 -- --------------------- m/ Z 94.00 21.42% m/z-> 60 70 80 90 100 110 120 130 140 150 160 170 180 190 Abundance #84500: DECADEUTEROPHENANTHRENE $$ Phenanthrene-d10 188

5000 22.40 22.60 22.80 23.00 23.20 80 94 m/z 80.05 16.36%

m/z-> 66 o1 ■ rM....... —IT ---------- 158

60 70 80 90 100 110 120 130 140 150 160 170 180 190 1.. Abundance #84499: Phenanthrene-d10 188 -' । ■ 11 । ■ 1 1 r ।1 ■ ■ ■ । 1 ■ ■ 1 । ■ 22.40 22.60 22.80 23.00 23.20 5000 m/z 189.10 15.06%

80 94 160 66 0 -HP - . ................. m/z-> 60 70 80 90 100 110 120 130 140 150 160 170 180 190 Abundance #84502: Anthracene-d10- ■ i ■ 1 1 ■ i ■ ' 1 rl 1 1 1 1 1 1 1 ' 1 1 ' 188 22.40 22.60 22.80 23.00 23.20 m/z 184.10 12.39%

5000

80 94 160 66

/z-> 0 r MP pr 60 -=Hmmmmm- 70 80 90 100 110 120 130 140 150 160 170 180 190 1041— — 2240 22.60 22.80 23.00 23.20

00462.D SCAN508.M Mon Jan 14 10:46:52 2002 Page 9

NYC-WTC_000051420

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NYC-WTC_000051420Source: NYC Law Department, mirrored locally

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