GCMS results for sample AE00462, Jan 24 2002

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Laboratory report showing GCMS analysis of sample AE00462 with surrogate recovery data on January 24, 2002.

NYC-WTC_000051408–000051421

Folder label: “GCMS X 1/8/02 A 1/11/02”

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NYC 9/11 Public Portal Document

Library Search Compound Report Data File : C:\MSDCHEM\1\5973N\02JAN11\00462.D Vial: 4 Acq On : 11 Jan 2002 4:36 pm Operator: Sample : 508 scan Inst : Instrumen Mise : January 11, 2002 Multiplr: 1.00 MS Integration Params: LSCINT.P Quant Method : C:\MSDCHEM\l-..\SCAN508.M (RTE Integrator) Title : 508 scan method Library : C:\DATABASE\WILEY7N. L ********************************************************************* Peak Number 6 4-METHOXY-.BETA.-METHYLCINN... Concentration Rank 6

R.T. EstConc Area Relative to ISTD R.T. 22.28 0.15 ug/L 89182 Phenanthrene-dl0 22.65 Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 4-METHOXY-.BETA.-METHYLCINNAMIC ... 192 C11H12O3 019169-94-9 64 2 N-perdeuteriobenzylideneaniline 192 C13D11N 000538-51-2 58 3 N-(2-methylprop-2-enyl)-2-nitrob... 192 C10H12N202 000000-00-0 49 4 1-amino-2-methyl-4-isopropyl-thi... 192 C5H13N4PS 107264-54-0 45 Abundance Scan 1656 (22.280 min): 00462. D (-) m/z 192.10 100.00% 192

5000

82 96 146 c 22.00 22.20 22.40 22.60 0 44 111 ■1 ■■ । ‘Er —DTTRPPTTmTT 70 I J 118 I 160 I+ m/z 191.10 16.75% /z—> 20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 200 Abundance #102588: 4-METHOXY-.BETA.-METHYLCINNAMIC ACID $$ 2-Butenoi... 192

108 5000 22.00 22.20 22.40 22.60 146 175 m/z 96.10 15.93% 0 • ■ i ■■■■i•■■* i ■ ■ ■ • t •■ ■ ■ i ■"'i" •'i■ ■" i ■ • r ' " i " " i " " i'1 ' r " ' i' " ■ i ■ .......... TTT n/z-> 20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 200 Abundance #88409: N-perdeuteriobenzylideneaniline 192 ..... ,....... II, 22.00 22 20 22.40 22.60 5000 82 m/z 146.10 15.44% 54 110 30 94 160 0 —TPTT TTTTT nPHP /z-> 20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 200 Abundance #102494: N-(2-methylprop-2-enyl)-2-nitrobenzenamine - 192 22.00 22.20 22.40 22.60 77 151 m/z 193.10 13.17% 130 93 104 5000 119

177 0 " i " " i " " i ■1" i1' ’' r ■ "i " ■ ■ i ‘ TT TT’T T‘T TTTT 1..... ' i1" ' r " 1 r " ' i " " i "I ' rT" 1 1 i 11 ■ 11 1 ' < I 1 । ' i ' m/z-> 20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 200 22.00 22.20 22.40 22.60

00462.D SCAN508.M Mon Jan 14 10:46:52 2002 Page 8

NYC-WTC_000051419

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NYC-WTC_000051419Source: NYC Law Department, mirrored locally

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