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GCMS blank results for sample AE03612, March 28, 2002

Machine-extracted title · confidence 90%

Laboratory report documenting GCMS analysis of a method blank for sample AE03612 to verify analytical system cleanliness.

NYC-WTC_000037720–000037739

Folder label: “GCMS X 2/19/02 A 3/8/02

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Scanned page image, NYC-WTC_000037738
OCR text

OCR status: ok · source: pdftotext

NYC 9/11 Public Portal Document

Library Search Compound Report Data File : C:\MSDCHEM\1\5973N\02MAR08\03612.D Vial: 2 Acq On : 8 Mar 2002 4:25 pm Operator: Sample : 508 scan Inst : Instrumen Mise : March 8, 2002 Multiplr: 1.00 MS Integration Params: LSCINT.P Quant Method : C:\MSDCHEM\1...\HP022102.M (RTE Integrator) Title : 508 scan method Library : C:\DATABASE\WILEY7N.L ********************************************************************* Peak Number 13 4-METHOXY-.BETA.-METHYLCINN... Concentration Rank 5

R.T. EstConc Area Relative to ISTD R.T.

22.28 0.13 ug/L 112372 Phenanthrene-dl0 22.63

Hit# of 5 Tentative ID MW MolForm CAS# Qual 1 4-METHOXY-.BETA.-METHYLCINNAMIC ... 192 C11H1203 019169-94-9 72 2 Phenanthrene, 9-methyl- $$ 9-Met... 192 C15H12 000883-20-5 50 3 N-(2-methylprop-2-enyl)-2-nitrob. .. 192 C10H12N2O2 000000-00-0 46 4 N-perdeuteriobenzylideneaniline 192 C13D11N 000538-51-2 45 Abundance Scan 1675 (22.283 min): 03512.D (-) m/z 192.00 100.00% 192

5000

146 > ■ i ■ ■ ■ •• r i ■ ■4 ■ i ■ ‘ 82 96 160 22.00 22.20 22.40 2260 66 miz-> 44 Of TIT TTTH1 -2 4... 11" 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 200 m/z 191.00 20.07% Abundance #102588: 4-METHOXY-BETA.-METHYLCINNAMIC ACID $$ 2-Butenoi... 192

108 5000 22.00 22.20 22.40 22.60 146 175 rn/z 146.10 17.69% 01 TI—Bpuu’, TBBTLnaur I ’ * 1111 ‘ j1 ‘ ‘ ‘ i ‘ ‘ Tf rrrrp-m I T ''■'I" "i‘ TIgr miz-> 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 200 Abundance #103936: Phenanthrene, 9-methyl-$$ 9-Methylphenanthrene 192 --------- 2200 22.20 22.40 22.60 5000 m/z96.00 13.70%

96 165 88 .1 139 152 ( 176 . 01 TII TTIgumpEmymmuf, T]r miz-> 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 200 Abundance #102494: N-(2-methylprop-2-enyl)-2-nitrobenzenamine 192 22.00 22.20 22.40 22.60 77 151 m/z 193.00 13.66% 130 93 104 5000 119

177 0 ‘ 1t i ■ ■1■i•••■i “ “ >■ ■ ■ ■ i “' i ■ Tp-r 1’’ ’11’ ’11’ 1 J •• ‘ I 1 1 1J l‘ 1 miz-> 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 200 22.00 22.20 22.40 22.60

03512.D HP022102.M Fri Mar 15 10:09:18 2002 Page 15

NYC-WTC_000037738

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NYC-WTC_000037738Source: NYC Law Department, mirrored locally

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