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GCMS analysis results for sample AE00319, Jan 2002

Machine-extracted title · confidence 100%

Laboratory report showing GCMS analysis of sample AE00319 for unknown compounds and DDD on January 10, 2002.

NYC-WTC_000051122–000051136

Folder label: “GCMS X 1/7/02 A 1/8/02

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Scanned page image, NYC-WTC_000051133
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NYC 9/11 Public Portal Document Library Search Compound Report

, Data File : C:\MSDCHEM\1\5973N\02JAN08\319.D Vial: 4 Acq On : 8 Jan 2002 7:56 pm Operator: Sample : 508scan Inst : Instrumen Mise : January 8, 2002 Multiplr: 1.00 MS Integration Params: LSCINT.P Quant Method : C:\MSDCHEM\1...\SCAN508.M (RTE Integrator) Title : 508 scan method Library : C:\DATABASE\WILEY7N.L ********************************************************************* Peak Number 6 4-METHOXY-.BETA.-METHYLCINN... Concentration Rank 7

R.T. EstConc Area Relative to ISTD R.T.

22.28 0.14 ug/L 84065 Phenanthrene-dl0 22.65

Hit# of 5 Tentative ID MW MolForm CAS# Qual 1 4-METHOXY-.BETA.-METHYLCINNAMIC ... 192 C11H1203 019169-94-9 72 2 Phenanthrene, 9-methyl- $$ 9-Met... 192 C15H12 000883-20-5 53 3 N-(2-methylprop-2-enyl)-2-nitrob... 192 C10H12N2O2 000000-00-0 46 4 l-amino-2-methyl-4-isopropyl-thi... 192 C5H13N4PS 107264-54-0 45 Abundance Scan 1656 (22.280 min): 319.D (-) m/z 192.10 100.00% 192

5000

TB 92 96 146 160 22.00 22.20 22.40 22.60

•n/z-> 49 OmPTT pHH 40 50 60 70 66 80 90 100 2L 118 ■......... * i' 110 ..... I.... I ' ' ' ' I 120 130 140 150 160 170 180 190 200 m/z 191.10 19.27% Abundance 1#102588: 4-METHOXY-.BETA.-METHYLCINNAMIC ACID $$ 2-Butenoi... 192

108 5000 22.00 22.20 22.40 22.60 146 175 m/z 146.10 13.67%

mlz-> 40 0T ' r ''' i' ■'' i ■''' i ■ 50 60 I' 1 1 ' I '' '' I ' ' ' I I " " I" " 11 Pi...... 70 80 90 100 110 120 130 140 150 160 170 180 190 200 u. Abundance #103936: Phenanthrene, 9-methyl- $$ 9-Methylphenanthrene 192 A i 1 ■ ■ ■ i 22.00 22.20 22.40 22.60 5000 m/z 193.10 13.58%

96 165 88 .il 139 152 ,| 176 . 0 i " ■ ’ i11 ■ ■ i'' " ■ i " ■11 ’111111111" '' 11 "' I " 1 ' 111" 11" ' I' i ■ ’1 ■ i1' ''i I Tp-1 m/z-> 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 200 Abundance #102494: N-(2-methylprop-2-enyl)-2-nitrobenzenamine ‘IT 192 22.00 22.20 22.40 22.60 77 130 151 m/z 96.10 13.25% 93 104 5000 119

177 0 i'' | ' i' ■' ■ r ■'' i1' "i ■ ■ •11 "ITT ‘1′1 T‘T TTI‘ ■ i' ■ ■ ■ i'' ' i ■ ■ ■ ■ i ■''' i ■ ■ i ■ > i 1 ’ ' 1 I /z-> 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 200 22.00 22.20 22.40 22.60

319.D SCAN508.M Wed Jan 09 15:17:57 2002 Page 8

NYC-WTC_000051133

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NYC-WTC_000051133Source: NYC Law Department, mirrored locally

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DEP GCMS data table, Jan-Feb 2002 · Box DEP Box 12

NYC-WTC_000004494

Multi-page laboratory data sheet containing sample analysis results and metadata for DEP GCMS records from January to February 2002.

1 shared non-person entities · 1 shared topics · similarity 0.996

machine-extracted · confidence unavailable · Check page ↗
DEP GCMS data table, Jan-Feb 2002 · Box DEP Box 12

NYC-WTC_000003981

Multi-page laboratory data sheet containing sample analysis results and metadata for DEP GCMS records from January to February 2002.

1 shared non-person entities · 1 shared topics · similarity 0.996

machine-extracted · confidence unavailable · Check page ↗

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