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← Document results/DEP Box 28/GCMS X 1/7/02 A 1/8/02
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GCMS analysis results for sample AE00319, Jan 2002

Machine-extracted title · confidence 100%

Laboratory report showing GCMS analysis of sample AE00319 for unknown compounds and DDD on January 10, 2002.

NYC-WTC_000051122–000051136

Folder label: “GCMS X 1/7/02 A 1/8/02”

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Scanned page image, NYC-WTC_000051132
OCR text

OCR status: ok · source: pdftotext

NYC 9/11 Public Portal Document Library Search Compound Report

Data File : C:\MSDCHEM\1\5973N\02JAN08\319.D Vial: 4 Acq On : 8 Jan 2002 7:56 pm Operator: Sample : 508scan Inst : Instrumen Mise : January 8, 2002 Multiplr: 1.00 MS Integration Params: LSCINT.P Quant Method : C:\MSDCHEM\1...\SCAN508.M (RTE Integrator) Title : 508 scan method Library : C:\DATABASE\WILEY7N.L ********************************************************************* Peak Number 5 3-(CYCLOHEX-3'-EN-YL)PROPAN... Concentration Rank 1

R.T. EstConc Area Relative to ISTD R.T.

5.89 5.01 ug/L 1734900 1,4-Dichlorobenzene-d4 9.72

Hit# of 5 Tentative ID MW MolForm CAS# Qual

13-(CYCLOHEX-3'-EN-YL)PROPANOL $$... 174 C8H14O4 015745-87-6(33 2 Acetic acid, 3-[1,3]dioxolan-2-y... 174 C8H14O4 000000-00-0 33 3 Silane, tetramethyl- $$ Tetramet... 88 C4H12Si 000075-76-3 25 4 Silane, tetramethyl- 88 C4H12Si 000075-76-3 25 Abundance Scan 220 (5.885 min): 319.D (-) m/z 73.10 100.00% 73

5000 43 5.60 5.80 6.00 6.20

m/z-> o 44458 1 87 103 , । rl ■ ■ । V < t'i 111.11।

10 20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 1111' 11 " ' i" ’ ■ i " 1' 11 "' I m/z 43.10 24.71% Abundance #36138: 3-(CYCLOHEX-3'-EN-YL)PROPANOL $$ 2-Cyclohexene-1-p...

5000 IIPIIT 5.60 5.80 6.00 6.20 43 m/ z 45.10 9.56% 27 55 87 113 174 o1 TVTTTTTTT T+ ri , I T1 Ip r " ' r ' ■' r " ' r '' ■ i ■ ■'' i l1 " ' I m/z-> 10 20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 Abundance #78238: Acetic acid, 3-[1,3]dioxolan-2-ylpropyl ester 73 5.60 5.80 6.00 6.20 5000 m/ z 41.10 9.16%

43 27 55 87 113 174 0V I'''11 T++ ii , 1 r liiyuidy i " " r ■ ■ ■ i " " i'' " i' " ' i i""r m/z-> 10 20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 Abundance #4812: Silane, tetramethyl- $$ Tetramethylsilane $$ (CH3)4... ■ i ■ ‘ 73 5.60 5.80 6.00 6.20 m/z 71.10 6.32%

5000

45 15 31 | 5588 0 " i" " i ■ " ' r TTTll" i1 ............... " r " 11 ■ i " ■ ■ i " ■ ■ i' ■ " r " ' i " " r " ■ I' ■ " i y Tl/Z-> 10 20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 5.60 5.80 6.00 6.20

319.D SCAN508.M Wed Jan 09 15:17:57 2002 Page 7

NYC-WTC_000051132

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NYC-WTC_000051132Source: NYC Law Department, mirrored locally

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DEP GCMS data table, Jan-Feb 2002 · Box DEP Box 12

NYC-WTC_000004494

Multi-page laboratory data sheet containing sample analysis results and metadata for DEP GCMS records from January to February 2002.

1 shared non-person entities · 1 shared topics · similarity 0.996

machine-extracted · confidence unavailable · Check page ↗
DEP GCMS data table, Jan-Feb 2002 · Box DEP Box 12

NYC-WTC_000003981

Multi-page laboratory data sheet containing sample analysis results and metadata for DEP GCMS records from January to February 2002.

1 shared non-person entities · 1 shared topics · similarity 0.996

machine-extracted · confidence unavailable · Check page ↗

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