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GCMS analysis results for sample AE00307, Jan 2002

Machine-extracted title · confidence 100%

Laboratory report showing GCMS analysis of sample AE00307 for unknown compounds and DDD on January 10, 2002.

NYC-WTC_000051055–000051072

Folder label: “GCMS X 1/7/02 A 1/8/02

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NYC 9/11 Public Portal Document

Library Search Compound Report Data File : C:\MSDCHEM\1\5973N\02JAN08\307.D Vial: 6 Acq On : 8 Jan 2002 9:37 pm Operator: Sample : 508scan Inst : Instrumen Mise : January 8, 2002 Multiplr: 1.00 MS Integration Params: LSCINT.P Quant Method : C:\MSDCHEM\1...\SCAN508.M (RTE Integrator) Title : 508 scan method Library : C:\DATABASE\WILEY7N.L ********************************************************************* Peak Number 6 3-(CYCLOHEX-3'-EN-YL)PROPAN. .. Concentration Rank 1 R.T. EstConc Area Relative to ISTD R.T. 5.89 5.05 ug/L 1668140 1,4-Dichlorobenzene-d4 9.72 Hit# of 5 Tentative ID MW MolForm CAS# Qual 13-(CYCLOHEX-3'-EN-YL)PROPANOL $$... 174 C8H14O4 015745-87-6 33 2 Acetic acid, 3-[1,3]dioxolan-2-y... 174 C8H14O4 000000-00-0 33 3 Silane, tetramethyl- $$ Tetramet... 88 C4H12Si 000075-76-3 25 4 Silane, tetramethyl- (CAS) $$ Te... 88 C4H12Si 000075-76-3 9 Abundance Scan 220 (5.885 min): 307.D (-) m/z 73.10 100.00% 73

5000

43 560 5.80 6.00 6.20

n/z-> 0- ITT’1 11 "1111 —ll 55 i1 '''‘'T ■ . , 87 103 । ' । ■'' ■ ।11' ■ । 10 20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 ‘I‘ m/z 43.10 24.01% Abundance #36138: 3-(CYCLOHEX-3'-EN-YL)PROPANOL $$ 2-Cyclohexene-1-p... 70

5000 . A j 5.60 5.80 6.00 6.20 43 m/z 45.10 9.45% 2755 87 113 174 OTTTTT PP 11" " 1...... .1 i i11'11 IP ।■■■>।■>■• ।■ ■■■ । I ■1 ■ ■ e n/z-> 10 20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 Abundance #78238: Acetic acid, 3-[1,3]dioxolan-2-ylpropyl ester 70

5.60 5.80 6.00 6.20 5000 m/z 41.10 8.70% 43 1 ! T I | _

27 87 o11' i " " r " ' i' mm In 55 , 113 174 n/z-> 10 20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 Abundance #4812: Silane, tetramethyl- $$ Tetramethylsilane $$ (CH3)4... 70 5.60 5.80 6.00 6.20 m/z 71.10 6.61% 5000

45 15 31 , I 55 OTrp’ . ।... 11'. TVTTTpmt | 88 ... . lesgtrstyssssprsssn-1*8g111*01*81018*G/G**GS/*SS** m/z-> 10 20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 5.60 5.80 6.00 6.20

307.D SCAN508 .M Wed Jan 09 15:16:56 2002 Page 8

NYC-WTC_000051066

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NYC-WTC_000051066Source: NYC Law Department, mirrored locally

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