GCMS analysis results for sample AE00307, Jan 2002

NYC 9/11 Public Portal Document

Llbrary Search Compound Report

Data File : C:\MSDCHEM\1\5973N\02JAN08\307.D Vial: 6 Acq On : 8 Jan 2002 9:37 pm Operator: Sample : 508scan Inst : Instrumen Mise : January 8, 2002 Multiplr: 1.00 MS Integration Params: LSCINT.P Quant Method : C:\MSDCHEM\1...\SCAN508.M (RTE Integrator) Title : 508 scan method Library : C:\DATABASE\WILEY7N.L ********************************************************************* Peak Number 5 3-PENTEN-2-OL, (Z)- Concentration Rank 10 R.T. EstConc Area Relative to ISTD R.T. 5.70 0.11 ug/L 36510 1,4-Dichlorobenzene-d4 9.72

Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 3-PENTEN-2-OL, (Z)- 86 C5H10O 024652-50-4/59 2 3-Penten-2-ol $$ .alpha.,.gamma... 86 C5H10O 001569-50-259 3 3-Penten-2-ol 86 C5H10O 001569-50-2 59 4 1-Trifluoroacetoxy-2-methylpentane 198 C8H13F302 000000-00-0 38 Abundance Scan 204 (5.703 min): 307. D (-) m/ z 41.10 100.00% 41 71

5000 45 nini prp Aer ,1, 51 58 86 5.40 5.60 5.80 6.00 m/z—> 01 4 m 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 1 i ■ ■ ■ ■ i ' ■ r 11 ' ■' ■ i' 1 — TTT m/z 43.10 92.62% Abundance #4208: 3-PENTEN-2-OL, (Z)- 7)1 43

5000 39 ‘E1‘ ' 1 i ■ ■ ■ ■ i ' 1 1 ■ i 53 67 5.40 5.60 5.80 6.00 27 m/z 71.10 69.96% 58 86

m/z-> 0 1' i '' ' ■ i ■ TTPTTH TTTT 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 14... all, I 95 '11l1, I■ y Abundance #4047: 3-Penten-2-ol $$ alpha., gamma.-Dimethylallyl alco... 43 71 ""I 5.40 5.60 5.80 6.00 5000 39 m/z 69.00 51.52% 27 53 67 58 86 - 49 m/z-> 0 ■ i - ■ ■ ■ i ■ 20 25 30 35 40 45 111'111 ■ ■ ■ ■ i' 50 55 60 65 TTt 70 I 75 80 85 90 95 Abundance #4046: 3-Penten-2-ol m/jj 71 5.40 5.60 5.80 6.00 43 m/z 39.10 41.46%

5000 39 53 67 27 58 86

m/z-> 0 1 ■ i' ■ ■ ■ i1 mPPTTTTT 20 25 30 35 W 40 45 TTTT 50 55 60 65 70 1 " 11 " 111 75 80 1 1' I' ■1 ■ i ■r 111

85 90 95 1 1 1 5.40 ,। । / ।,. n. 5.60 5.80 6.00

307.D SCAN508.M Wed Jan 09 15:16:56 2002 Page 7

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