GCMS analysis results for sample AE00307, Jan 2002

NYC 9/11 Public Portal Document

Llprary searcn compound Keporc Data File : C:\MSDCHEM\1\5973N\02JAN08\307.D Vial: 6 Acq On : 8 J an 2002 9:37 pm Operator: Sample : 508scan Inst : Instrumen Mise : January 8, 2002 Multiplr: 1.00 MS Integration Params: LSCINT.P Quant Method : C:\MSDCHEM\l-..\SCAN508.M (RTE Integrator) Title : 508 scan method Library : C:\DATABASE\WILEY7N. L ********************************************************************* Peak Number 4 Butenol, methyl- Concentration Rank 7

R.T. EstConc Area Relative to ISTD R.T. 5.01 0.16 ug/L 52238 1,4-Dichlorobenzene-d4 9.72

Hit# of 5 Tentative ID MW MolForm CAS# Qual 1 Butenol, methyl- 86 C5H10O 060766-00-9(64 2 2-Furanmethanol, tetrahydro- (CA... 102 C5H10O2 000097-99-4 59 3 3-hydroxy-4,4-dimethyl .gamma. B. . . 130 C6H10O3 052126-90-6 42 4 3-Buten-2-ol, 2-methyl- 86 C5H10O 000115-18-4 39 Abundance Scan 143 (5.006 min): 307. D (-) m/z 71.10 100.00% 43 71

5000 39 55 59 1 X .111I।।

n/z-> 5 Or ■ ■ I ■ ■1' i' ■ ■ ■ i'' ■' i'' ■ ■ r ■111 ■ AlL. 10 15 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 । 51 , 86 *I}mu——p‘uutu"n‘t 4 60 m/z 4.80 43.10 5.00 5.20 5.40 92.27% Abundance #4093: Butenol, methyl- 43 71

5000 27 59 AAAt 4.60 4.80 5.00 5.20 5.40 15 31 m/z 41.10 66.96% 53 ■ A /z-> Of TITT ITTTTI’I’ TTI '11 " " I ..I1 - 5 10 15 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 4 67.

Abundance #9384: 2-Furanmethanol, tetrahydro- (CAS) $$ Tetrahydrofur... 7h 43 4.60 4.80 5.00 5.20 5.40 5000 27 m/ z 69.10 51.63% 31

Of ‘ I 37 m 1....... 4 111'11 m/z-> 5 10 15 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 Abundance #26149:3-hydroxy-4,4-dimethyl .gamma. Butanolactone $$ Pa... —-rT-r-r-r-r-p-r- ' i r 1 ' ' i ■ 7h 4.60 4.80 5.00 5.20 5.40 43 m/z 59.10 37.87%

5000

31 68

/z-> 0b ■11 ■1'11' 11" ' J1" i " " i — —mmmmmmmmP 5 10 15 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 -A — poh/pii. ) 4.60 4.80 5.00 5.20 5.40

307.D SCAN508.M Wed Jan 09 15:16:56 2002 Page 6

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