Laboratory report documenting a method blank analysis to verify absence of contamination during gas chromatography-mass spectrometry testing.
NYC-WTC_000051353–000051363Folder label: “GCMS X 1/8/02 A 1/11/02”
OCR status: ok · source: pdftotext
NYC 9/11 Public Portal Document
Library searcn compound Keporc
Data File : C:\MSDCHEM\1\5973N\02JAN14\0108BA.D Vial: 1 Acq On : 14 Jan 2002 10:28 am Operator: Sample : lab blank 1/8 a Inst : Instrumen Mise : January 14, 2002 Multiplr: 1.00 MS Integration Params: LSCINT.P Quant Method : C:\MSDCHEM\1...\SCAN508.M (RTE Integrator) Title : 508 scan method Library : C:\DATABASE\WILEY7N.L ********************************************************************* Peak Number 1 2-Butenal, 3-methyl- (CAS) ... Concentration Rank 3
R.T. EstConc Area Relative to ISTD R.T.
4.84 0.24 ug/L 69729 1,4-Dichlorobenzene-d4 9.72
Hit# of 5 Tentative ID MW MolForm CAS# Qual
1 2-Butenal, 3-methyl- (CAS) $$ 3-... 84 C5H80 000107-86-8 64 2 2-Butenal, 3-methyl- $$ Crotonal... 84 C5H80 000107-86-8 64 3 Furan, 2,3-dihydro-4-methyl- (CA... 84 C5H8O 034314-83-5 59 4 2-Butenal, 3-methyl- 84 C5H80 000107-86-8 53 Abundance Scan 128 (4.835 min): 0108BA. D (-) m/z 84.05 100.00% 84
55 5000 41 59 51 36 ...... 4.40 4.60 4.80 5.00 5.20 01 ■ i ■ ■ ------ ■ i ■11 ■ i1 m/ z 55.10 60.66% m/z-> 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 Abundance #3221:2-Butenal, 3-methyl- (CAS) $$ 3-Methyl-2-butenal 84 55
39 5000 27 4.40 4.60 4.80 5.00 5.20 m/ z 83.10 47.27%
n/z-> Of ■111 ■1 ■ i1 TPTTH ++ lamm— 0- 44 51 1
20 25 30 35 40 45 50 55 60 65 70 75 80 85 69 111 ■'111 90 Abundance #3222: 2-Butenal, 3-methyl- $$ Crotonaldehyde, 3-methyl- $... 84 55 4.40 4.60 4.80 5.00 5.20 39 m/z 41.10 44.06% 5000 27
m/z-> +ZHH 01 ■ । ■ ■ ■ ■ । > ■ i ■ ■ ■ • i' I ■ 20 25 30 35 40 45 50 55 60 65 70 75 80 85 69 HTP ■ i' ' ' 1 i 90 ..................................................... . ................. ■■■■ Abundance #3351: Furan, 2,3-dihydro-4-methyl- (CAS) $$ 4-METHYL-2,3-. 56 84 4.40 4.60 4.80 5.00 5.20 m/z 59.00 41.68%
5000 41
m/z-> 0 20 25 30 35 40 44 45 51
50 55 >11 ■1 >111 > ■ 11 ■ > ■ ■ l ■ । ■ t • •
60 65 69
70 75 80 —85PPP 90 ... 4.40 4.60 4.80 A 5.00 5.20
0108BA.D SCAN508.M Tue Jan 15 08:47:57 2002 Page 3
NYC-WTC_000051358
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NYC-WTC_000049891
Laboratory report showing blank analysis results with concentrations below method detection limits for various organic compounds.
1 shared non-person entities · 1 shared topics · Same agency, volume and box · similarity 0.995
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000051055
Laboratory report showing GCMS analysis of sample AE00307 for unknown compounds and DDD on January 10, 2002.
1 shared non-person entities · 1 shared topics · Same agency, volume and box · similarity 0.993
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000051088
Laboratory report showing GCMS analysis of sample AE00309 for unknown compounds and DDD on January 10, 2002.
1 shared non-person entities · 1 shared topics · Same agency, volume and box · similarity 0.993
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000051040
Laboratory report showing GCMS analysis of sample AE00276 for unknown compounds and DDD on January 10, 2002.
1 shared non-person entities · 1 shared topics · Same agency, volume and box · similarity 0.993
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000049929
Laboratory report showing GCMS analysis of sample AD31637 including unknown compounds and surrogate recovery data.
1 shared non-person entities · 1 shared topics · Same agency, volume and box · similarity 0.992
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000051073
Laboratory report showing GCMS analysis of sample AE00308 for unknown compounds and DDD on January 10, 2002.
1 shared topics · Same agency, volume and box · similarity 0.992
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000051422
Laboratory report showing GCMS analysis of sample AE00463 with surrogate recovery data on January 24, 2002.
1 shared topics · Same agency, volume and box · similarity 0.992
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000051010
Blank analysis report for GCMS of sample AE00275 showing compounds below method detection limits from January 8-10, 2002.
1 shared non-person entities · 1 shared topics · Same agency, volume and box · similarity 0.992
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000051471
Laboratory report showing GCMS analysis of sample AE00469 with surrogate recovery data on January 24, 2002.
1 shared topics · Same agency, volume and box · similarity 0.992
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000051137
Laboratory report showing GCMS analysis of sample AE00320 for unknown compounds and DDD on January 10, 2002.
1 shared topics · Same agency, volume and box · similarity 0.992
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000051439
Laboratory report showing GCMS analysis of sample AE00464 with surrogate recovery data on January 24, 2002.
1 shared non-person entities · 1 shared topics · Same agency, volume and box · similarity 0.992
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000049916
Laboratory report showing GCMS analysis of sample AD31631 including unknown compounds and surrogate recovery data.
1 shared topics · Same agency, volume and box · similarity 0.992
machine-extracted · confidence unavailable · Check page ↗No available related records indexed in this group.
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NYC-WTC_000051336
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NYC-WTC_000051337
Administrative label page identifying the folder range for gas chromatography-mass spectrometry records from January 8 to January 11, 2002.
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NYC-WTC_000051338
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NYC-WTC_000051340
Laboratory report listing concentrations of volatile organic compounds including nitrosamines and chlorinated solvents in sample AE00314.
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NYC-WTC_000051344
Second calibration standard report for gas chromatography-mass spectrometry analysis of sample AE00314 conducted on January 15, 2002.
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