GCMS analysis results for sample AE00309, Jan 2002

NYC 9/11 Public Portal Document

Llprary searcn Compound Report

Data File : C:\MSDCHEM\1\5973N\O2 JAN08\309.D Vial: 8 1 Acq On : 8 Jan 2002 11:19 pm Operator: Sample : 508scan Inst : Instrumen Mise : January 8, 2002 Multiplr: 1.00 MS Integration Params: LSCINT.P Quant Method : C:\MSDCHEM\1...\SCAN508.M (RTE Integrator) Title : 508 scan method Library : C:\DATABASE\WILEY7N.L ********************************************************************* Peak Number 4 2-Furanmethanol, tetrahydro... Concentration Rank 7

R.T. EstConc Area Relative to ISTD R.T. 5.01 0.13 ug/L 41048 1,4-Dichlorobenzene-d4 9.72 Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 2-Furanmethanol, tetrahydro- (CA... 102 C5H10O2 000097-99-4 738 2 Butenol, methyl- 86 C5H10O 060766-00-9 36 3 3-Buten-2-ol, 2-methyl- (CAS) $$... 86 C5H10O 000115-18-4 36 4 2-Pentene, 3-methyl-, (Z)- $$ (Z... 84 C6H12 000922-62-3 14 Abundance Scan 143 (5.006 min): 309. D (-) m/z 71.10 100.00% 41 71

5000

44 55 59 M Or — TTT 84 1ll.5t 4.60 m/ z 4.80 41.10 5.00 5.20 5.40 79.63% I ■ ■ i ■ ■ ■ ■ i1 ■ ■ ■ i ■' ■ ■ i ■'1 ■ i ■1 ■11 ■ ■

m/z-> 5 10 15 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 Abundance #9384: 2-Furanmethanol, tetrahydro- (CAS) $$ Tetrahydrofur... 7h 43

5000 27 31 4.60 4.80 5.00 .0,4.7.. 5.20 5.40 m/z 43.10 71.41%

n/z-> Of 5 1 ■ r ■ " i ■ ■1 ■ r " ■ r TTT 7 37

10 15 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 53 „ , I 57 61 --H + TT A Abundance #4093: Butenol, methyl- 43 71 AMW, AAA, 460 4.80 5.00 5.20 5.40 5000 59 m/z 69.10 56.15% 27 15 31 53 i"11111U" 11 67, 86 m/z-> Or 111 ■1 1’1’11111 "II 1" r " ' i i1" ' i " " i 5 10 15 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 .. I Abundance #4081: 3-Buten-2-ol, 2-methyl- (CAS) $$ 2-Methyl-3-buten-2... A_ 7h 4.60 4.80 5.00 5.20 5.40 m/ z 59.10 33.57% 43 5000 59 27 31 53 67

m/z-> Or 5 10 15 20 25 H 30 40 4 50 mnMH 35 65 H. ........ 90 .TTTT 45 55 60 70 75 80 85 —A—A 4.60 4.80 5.00 5.20 5.40

309.D SCAN508.M Wed Jan 09 15:17:25 2002 Page 6

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