GCMS analysis results for sample AE00309, Jan 2002

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Laboratory report showing GCMS analysis of sample AE00309 for unknown compounds and DDD on January 10, 2002.

NYC-WTC_000051088–000051104

Folder label: “GCMS X 1/7/02 A 1/8/02”

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NYC 9/11 Public Portal Document

' Acq On Mise Title Library Abundance ulprary searcn compound Report Data File : C : \MSDCHEM\1\5973N\02JAN08\309 . D Vial: 8 : 8 Jan 2002 11:19 pm Operator: Sample : 508scan Inst : Instrumen : January 8, 2002 Multiplr: 1.00 MS Integration Params: LSCINT.P Quant Method : C:\MSDCHEM\l-..\SCAN508.M (RTE Integrator) : 508 scan method : C:\DATABASE\WILEY7N.L ********************************************************************* Peak Number 5 Cyclopropanecarboxylic acid... Concentration Rank 9 R.T. EstConc Area Relative to ISTD R.T. 5.70 0.10 ug/L 32348 1,4-Dichlorobenzene-d4 9.72 Hit# of 5 Tentative ID MW MolForm CAS# Qual 1 Cyclopropanecarboxylic acid (CAS... 86 C4H6O2 001759-53-1 43) 2 (IRS,5SR)-2,2,5-trimethylcyclope ... 140 C9H16O 122052-80-6 37/ 3 4-METHOXY-2-BUTEN-1-OL $$ 2-Bute... 102 C5H10O2 026089-32-7 28 4 3-Penten-2-ol (CAS) $ $ 2 -PENTEN- ...86 C5H100 001569-50-2 25 Scan 204 (5.703 min): 309.D (-) m/z 41.10 100.00% 41 71

5000

Pin । । Y 1MItu Pu । । <A_I ___ । । 11 84 5.40 5.60 5.80 6.00 0 m/z 43.10 80.91% 80 1 9o' ioo iio "l20 130 140 ' I 1 1 1 ' i ' ' ' ■ i' ■ ■ ■ । ■

/z-> 20 30 40 50 60 70 Abundance #3764: Cyclopropanecarboxylic acid (CAS) $$ Carboxycyclopr... 30

5000 85 - I l py - Ki —■ ' 1 1 I ' ' 1 45 58 5.40 5.60 5.80> 6.00 27 68 m/z 71.10 72.19%

Tl/Z--> 0+ l.44 20 30 40 — 50 60 1.............ll............................................................ i ■ 1 ■ ■ i • 1 1 1 1 1 • 1 ■ i ■ ■ 1 1 i ■ ■ ■ 1 i ■ ' 1 1 i ■ ■ ■ ■ i ■ ■ 70 80 90 100 110 120 130 140 Abundance #36214: (1 RS,5SR)-2,2,5-trimethylcyclopentane-1-carbaldehy... 41 71 55 011 T 1 1 put । ' | 5.40 5.60 5.80 6.00 5000 m/z 39.10 50.70% 84 . . . rr | > ! I I | I 140 0+ m/z-> 20 30 40 50 60 70 80 90 100 110 120 130 140 Abundance #9336: 4-METHOXY-2-BUTEN-1-OL $$ 2-Buten-1-ol, 4-methoxy- ... ........... Ail, ' 1 ’ 1 41 5.40 5.60 5.80 6.00 71 m/ z 69.10 42.16% 5000 31 53 84 60

m/z-> 0 ■ i' ' ' ' i r'' ■’T111 1 11 ! 111 । । 11'pi*TIIT 20 30 40 50 60 70I 80 90 100 110 120 130 140 p...................... 540 5.60 5.80 6.00

309.D SCAN508.M Wed Jan 09 15:17:26 2002 Page 7

NYC-WTC_000051098

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NYC-WTC_000051073

Laboratory report showing GCMS analysis of sample AE00308 for unknown compounds and DDD on January 10, 2002.

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