GCMS results for sample AE00463, Jan 24 2002

NYC 9/11 Public Portal Document

ulprary searcn Compound Report

Data File : C:\MSDCHEM\1\5973N\02JAN11\00463.D Vial: 5 Acq On : 11 Jan 2002 5:25 pm Operator: Sample : 508 scan Inst : Instrumen Mise : January 11, 2002 Multiplr: 1.00 MS Integration Params: LSCINT.P Quant Method : C:\MSDCHEM\1...\SCAN508.M (RTE Integrator) Title : 508 scan method Library : C:\DATABASE\WILEY7N.L ********************************************************************* Peak Number 3 CIS-1-METHOXY-2-BUTENE Concentration Rank 5 R.T. EstConc Area Relative to ISTD R.T. 5.70 0.23 ug/L 70724 1,4-Dichlorobenzene-d4 9.72

Hit# of 5 Tentative ID MW MolForm CAS# Qual

I CIS-1-METHOXY-2-BUTENE 86 C5H10O 010034-14-7 58 2 2-Butene, 1-methoxy-, (Z)- 86 C5H10O 010034-16-9 53 3 3-Penten-2-ol 86 C5H10O 001569-50-2 45 4 3-PENTEN-2-OL, (Z) -_______________ 86 C5H10O 024652-50-4 45 Abundance Scan 204 (5.703 min): 00463.D (-) m/z 41.10 100.00% 41 71

5000 45 53 58 84 ■ ■ ■ i • ■ -A m/z-> 01 20 11 ■ ■ ■ ■ i ■ ■ ■ ‘ 11'1111 25 30 35 lilli.k,. T,".... lil 40 45 50 55 60 65 70 75 - 80 85 90 95 m/z 5.40 5.60 43.10 5.80 6.00 94.87% Abundance #4111: CIS-1-METHOXY-2-BUTENE 71 27 39 5000 55 ‘ ‘I’’ 1100* IIv . . . । 5.40 5.60 5.80 6.00 45 m/ z 71.10 86 90.92% 51 0 ■ i' ■ ■r । ■ 20 25 33 ■ ■ । 1 ■ 11 ।1 ■ 1’1 - +59, ■ i '' ' ■ i I"'......... ■'111 > 111 >'1 ■ I m/z-> 30 35 40 45 50 55 60 65 70 75 80 85 90 95 Abundance #4207: 2-Butene, 1-methoxy-, (Z)- 71 27 ... .A . , „ ! | 5,40 5.60 5.80 6.00 39 5000 55 m/z 69.00 42.52% 45 86 33 51 Of ' '7 1' 1 ' I ' TTTTTTTTT TTT - 20 25 30 35 40 45 50 55 60 65 158........70 ........ Pr 75 80 85 90 95 1 ‘ I ''1' I Ti/Z—> Abundance #4046: 3-Penten-2-ol 71 -A 5.40 5.60 5.80 6.00 43 m/z 39.10 .42.08%

5000 39 53 67 27

m/z-> 0 1' I''' ‘ i' 20 25 ■111 TTT 30 35 + al... + -H 40 45 TIIT 50 55 58

60 65 70 75 80 86

85 90 95 ' 1TT 1 540 5.60 5.80 6.00 TI

00463.D SCAN508.M Mon Jan 14 10:46:56 2002 Page 5

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