GCMS analysis results for sample AE00110, Feb 2002

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Laboratory report listing unknown compounds and surrogate recovery for sample AE00110 analyzed on February 13, 2002.

NYC-WTC_000050645–000050663

Folder label: “GCMS X 1/4/02 A 2/4/02”

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NYC 9/11 Public Portal Document ulbrary searcn compound Report

Data File : C:\MSDCHEM\1\5973N\02FEB04\00110.D Vial: 4 • Acq On 4 Feb 2002 1:28 pm Operator: Sample : 508 scan Inst : Instrumen Mise : February 4, 2002 Multiplr: 1.00 MS Integration Params: LSCINT.P Quant Method : C:\MSDCHEM\1... \SCAN508.M (RTE Integrator) Title : 508 scan method Library : C:\DATABASE\WILEY7N.L ********************************************************************* Peak Number 3 2-Buten-l-ol, 2-methyl- (CA... Concentration Rank 9 R.T. EstConc Area Relative to ISTD R.T. 4.62 0.11 ug/L 58156 1,4-Dichlorobenzene-d4 9.72 Hit# of 5 Tentative ID MW MolForm - CAS# Qual 1 2-Buten-l-ol, 2-methyl- (CAS) $$... 86 C5H10O 004675-87-0 50 2 2-Buten-l-ol, 3-methyl- (CAS) $$... 86 C5H10O 000556-82-1 49 3 2-Buten-l-ol, 3-methyl- $$ .gamm... 86 C5H10O 000556-82-1 47 4 2-Buten-l-ol, 3-methyl- 86 C5H10O 000556-82-1 38 Abundance Scan 109 (4.618 min): 00110.D (-) m/z 71.10 100.00% 71 41 57 88

... ANA.) 5000 53 85 14 68 4.20 4.40 4.60 4.80 5.00 Of **1010111011321033 -p-rr-r-p-T I ‘ ‘ 1 ‘ I ' ’81 mmM -rp-n-rp-r m/z 41.10 77.79% niz-> 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 Abundance #4064:2-Buten-1-ol, 2-methyl- (CAS) $$ 2-Methyl-but-2-ene... 71 N.... . 5000 43 86 A/i ■ ■ ■ ■ i ' 4.20 4.40 4.60 4.80 5.00 39 53 m/z 57.10 56.39% 57 67

m/z-> 0 ■n-p i i i p > ri p i i i p i • !•>•• 11 • 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 ...7.... Hu ajunasga TI 1' ■ i •1111 Abundance #4075: 2-Buten-1-ol, 3-methyl- (CAS) $$ Prenol $$ 2-METHYL... 71 41 I ■ ‘ ‘ I 1 ' 1 ' I ‘ ' I ‘ ' 11B 4.20 4.40 4.60 4.80 5.00 5000 m/z 88.00 53.89% 53 86 67 83, Of ' ■ i “ ■ ■ i “ 111■■■■i‘11 TT-p-n-rp- 113 *% --- -rp-n-rp-r n/z-> 20 25 303540455055 60 65 70 80 85 90 95 Abundance #4067:2-Buten-1-ol, 3-methyl- $$.gamma.,.gamma.-Dimethyl... । ■ i • ■ ■ ■ i > •' • । ■ • ■ ■ । • 71 4.20 4.40 4.60 4.80 5.00 m/z 43.10 52.71% 5000 53 27

1 As , A . 86 31 67 0 " i ■ ■ ■ ■ i' ’ T " i “ ■' i ■ “ ■ i ■ TT 59 TIH . J 11111"11'"11 11 • t ■ • * ■ । • /z—> 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 4.20 4.40 4.60 4.80 5.00

>0110.0 SCAN508.M Tue Feb 05 09:47:01 2002 Page 5

NYC-WTC_000050653

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