GCMS analysis results for sample AD31631, Jan 28 2002

NYC 9/11 Public Portal Document Library Searcn Compound Report

Data File : C:\MSDCHEM\l\5973N\02JAN17\31631.D Vial: 3 * Acq On : 17 Jan 2002 11:52 am Operator: Sample : 508 scan Inst : Instrumen Mise : January 17, 2002 Multiplr: 1.00 MS Integration Params: LSCINT.P Quant Method : C:\MSDCHEM\1.. .\SCAN508.M (RTE Integrator) Title : 508 scan method Library : C:\DATABASE\WILEY7N.L ********************************************************************* Peak Number 3 3-Buten-2-ol, 2-methyl- Concentration Rank 6

R.T. EstConc Area Relative to ISTD R.T. 4.99 0.11 ug/L 31458 1,4-Dichlorobenzene-d4 9.71 Hit# Of 5 Tentative ID MW MolForm CAS# Qual

1 3-Buten-2-ol, 2-methyl- 86 C5H10O 000115-18-4 56 2 3-Buten-2-ol, 2-methyl- (CAS) $$... 86 C5H10O 000115-18-4 50 3 (E)-5-Methyl-2-methylene-2-hexen... 126 C8H140 000000-00-0 10 4 3-Buten-2-ol, 2-methyl- (CAS) $$... 86 C5H10O 000115-18-4 9 Abundance Scan 142 (4.995 min): 31631.0 (-) m/z 43.10 100.00% 43 71

5000 59

49 T-1 •’ । 1 1' 1,1 '"I 1 '■ 86 4.60 4.80 5.00 5.20 5.40 Of T ' I" ‘ p-rr l1 ' ‘ 'I ‘ ' T ।111...j।।. m/z 71.10 98.79% mfe-> 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 100105110 Abundance #4084:3-Buten-2-ol, 2-methyl- 43 7h1

5000 I ll . -r-rp-r-r-r-rp-r-r 59 4.60 4.80 5.00 5.20 5.40 m/z 41.10 48.31% 27 53 , 86 ।11■11 11111111 Of mHHH iz-> 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 100105110 Abundance #4086:3-Buten-2-ol, 2-methyl- (CAS) $$ 2-Methyl-3-buten-2... 43 71 59 4.60 4.80 5.66 5.20 5.40 5000 m/z 69.10 44.85%

27 54 86

n/z-> 0 12011122010 Tp+T HH 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 100 105110 Abundance #23067: (E)-5-Methyl-2-methytene-2-h®<en-1-ol • ।t।।j * • 43 4.60 4.80 5.00 5.20 5.40 m/z 59.10 39.57%

50)0 59

49 84

miz-> 0 ।j...i,. p-rrrp-r ,.... ।. t.... । k. I. j. 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 100 105 110 r । 4.60 ■ whA. 4.80 5.00 5.20 5.40

31631.D SCAN508.M Tue Jan 22 08:36:55 2002 Page 5

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