GCMS analysis results for sample AD31631, Jan 28 2002

NYC 9/11 Public Portal Document Library Search Compound Report Data File : C:\MSDCHEM\1\5973N\02JAN17 31631.D Vial: 3 Acq On : 17 Jan 2002 11:52 am Operator: Sample : 508 scan Inst : Instrumen Mise : January 17, 2002 Multiplr: 1.00 MS Integration Params: LSCINT.P Quant Method : C:\MSDCHEM\1...\SCAN508. M (RTE Integrator) Title : 508 scan method Library : C:\DATABASE\WILEY7N.L ********************************************************************* Peak Number 4 Acetic acid, 3-[1,3]dioxola... Concentration Rank 1 R.T. EstConc Area Relative to ISTD R.T. 5.89 4.71 ug/L 1378700 1,4-Dichlorobenzene-d4 9.71 Hit# of 5 Tentative ID MW MolForm CAS# Qual 1 Acetic acid, 3-[1,3]dioxolan-2-y... 174 C8H14O4 000000-00-0 33 2 3-(CYCLOHEX-3'-EN-YL)PROPANOL $$... 174 C8H1404 015745-87-6 33 3 N-Ethylformamide $$ N-Formylethy. . . 73 C3H7NO 000627-45-2 9' 4 1,3-Dioxolane, 2-heptyl-172 C10H20O2 004359-57-3 9 Abundance Scan 220 (5.885 min): 31631 .D (-) m/z 73.10 100.00% 73

5000- 43

,1.1 55 11 87 । 103 । ' 5.60 5.80 6.00 6.20 0 ‘ 11 “ > 111 ‘111 ■ 1 . (I’ll . 1 . 1" । । > 1 .. । I । n . I ।.. i I । ।. m/z 43.10 23.84% z-> 10 20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 Abundance #78238: Acetic acid, 3-[1,3]dioxolan-2-ylpropyl ester 73

5000 m . i I—— . 5.60 5.80 6.00 6.20 43 m/z 45.10 9.09% 27 55 ,i , 87 113 174 0-—pmpm 11 ■" ■ i•“ ‘B 1a-paah-p—da*)****p"t*m l“ 11111'111 ri 111111111111111111 niz-> 10 20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 Abundance #36138:3-(CYCLOHEX-3'-EN-YL)PROPANOL $$ 2-Cyclohexene-1-p... 73 1 1 I" ' 5.60 5.80 6.00 6.20 5000 m/z 41.10 8.88% 43 27 55... J , 87 113 174 0- ■ • i ■ ■ “ i "111"11'1 ’1+4+1*34318 m/z-> 10 20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 Abundance #1794: N-Ethylformamide $$ N-Formylethylamine $$ Formamide... "* I 1 —m—mr 30 5.60 5.80 6.00 6.20 73 m/z 71.10 6.63% 5000- 44 58

15 0— nil ... TOIuaOgOa—PTPDTTTTT IIIIAfPI1I+114411 miz—> 10 20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 5.60 5.80 6.00 6.20

31631.D SCAN508.M Tue Jan 22 08:36:55 2002 Page 6

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