GCMS analysis results for sample AD31631, Jan 28 2002

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Laboratory report showing GCMS analysis of sample AD31631 including unknown compounds and surrogate recovery data.

NYC-WTC_000049916–000049928

Folder label: “GCMS X 1/3/02 A 1/17/02”

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NYC 9/11 Public Portal Document Llbrary searcn compound Report Data File : C:\MSDCHEM\1\5973N\02JAN17\31631.D Vial: 3 * Acq On : 17 Jan 2002 11:52 am Operator: Sample : 508 scan Inst : Instrumen Mise : January 17, 2002 Multiplr: 1.00 MS Integration Params: LSCINT.P Quant Method : C:\MSDCHEM\1...\SCAN508.M (RTE Integrator) Title : 508 scan method Library : C:\DATABASE\WILEY7N.L ********************************************************************* Peak Number 5 4-METHOXY-.BETA.-METHYLCINN... Concentration Rank 5 R.T. EstConc Area Relative to ISTD R.T. 22.28 0.13 ug/L 66901 Phenanthrene-dl0 22.63 Hit# of 5 Tentative ID MW MolForm CAS# Qual 1 4-METHOXY-.BETA.-METHYLCINNAMIC ... 192 C11H1203 019169-94-9 72 2 N-perdeuteriobenzylideneaniline 192 C13D11N 000538-51-2 64 3 Phenanthrene, 9-methyl- $$ 9-Met... 192 C15H12 000883-20-5 59 4 N-(2-methylprop-2-enyl)-2-nitrob... 192 C10H12N2O2 000000-00-0 52 Abundance Scan 1656 (22.280 min): 31631 .D (-) m/z 192.10 100.00% 1912

5000 .................................. / \ 146 160 22.00 22.20 22.40 '22^0 0 “■। 66 । ■ • ■ • । ■ ■ ■ ■ । ■ ■' ■ ।' ...................... ..... “ I'''' I' Tp m/z 191.10 15.49% m/z—> 20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 200 Abundance #102588:4-METHOXY-.BETA-METHYLCINNAMIC ACID $$ 2-Butenoi... 192

108 5000 ‘22M 22.20 22.40 22.60 146 175 m/z 193.10 14.70%

miz—> 0’ ... t. ।. ।, 1111111111 i-i 11111111111111111 ri I'''' I''' ‘ I ‘“ I ‘ ‘ 20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 200 ■ I ‘" I' ‘ “ I' '!■' “I1 U Abundance #88409: N-perdeuteriobenzylideneaniline 192

22.00 22.20 22.40 22.60 5000 82 m/z 160.10 14,25%

54 110

m/z—> 0 m 30 > • । • > > ■ । • -HP Tmmmppt 1 94 160 20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 200 4 Abundance #103936: Phenanthrene, 9-methyl- $$ 9-Methylphenanthrene । | 11-1 . | I , 1 , { I V-T T 192 22.00 22.20 22.40 22.60 m/z 146.10 13.73%

5000

88 T 139 152 155 176 _ ( 0 1111 । > >, > > > 1111111111111 171 1111 | 111111 H 111 n 11 n 11 | 1111111. i'| 111111 n 111'1'111 n 1111 r’r .............. ■ । ‘ / ■ 11 ■1 ‘ 11 11 /z—> 20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 200 22.00 22.20 22.40 22.60

31631.D SCAN508.M Tue Jan 22 08:36:55 2002 Page 7

NYC-WTC_000049926

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NYC-WTC_000049926Source: NYC Law Department, mirrored locally

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GCMS analysis results for sample AD31671, Jan 28 2002 · Box DEP Box 28

NYC-WTC_000050024

Laboratory report showing GCMS analysis of sample AD31671 including unknown compounds and surrogate recovery data.

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