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GCMS analysis results for sample AE00165, Feb 2002

Machine-extracted title · confidence 100%

Laboratory report listing unknown compounds and surrogate recovery for sample AE00165 analyzed on February 13, 2002.

NYC-WTC_000050664–000050682

Folder label: “GCMS X 1/4/02 A 2/4/02

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NYC 9/11 Public Portal Document Library searcn compound Report

Data. File : C : \MSDCHEM\1\5973N\02FEB04\ 00165 .D Vial: 4 • Acq On : 4 Feb 2002 5:37 pm Operator: Sample : 508 scan Inst : Instrumen Mise : February 4, 2002 Multiplr: 1.00 MS Integration Params: LSCINT.P Quant Method : C:\MSDCHEM\1... \SCAN508.M (RTE Integrator) Title : 508 scan method Library : C:\DATABASE\WILEY7N.L ********************************************************************* Peak Number 11 4-METHOXY-.BETA.-METHYLCINN... Concentration Rank 5 R.T. EstConc Area Relative to ISTD R.T.

22.28 0.15 ug/L 122673 Phenanthrene- dl 0 22.65

Hit# of 5 Tentative ID MW MolForm CAS# Qual 1 4-METHOXY-.BETA.-METHYLCINNAMIC ... 192 C11H1203 019169-94-9 72 2 3-Cyanocarbazole $$ 9H-Carbazole... 192 C13H8N2 057102-93-9 64 3 Phenanthrene, 9-methyl- $$ 9-Met... 192 C15H12 000883-20-5 59 4 N-perdeuteriobenzylideneaniline 192 C13D11N 000538-51-2 53 Abundance Scan 1656 (22.280 min): 00165. D (-) m/z 192.10 100.00% 1912

5000

40 70 82 96 146 160 S 22.00 22.20 22.40 22.60 0- -PPH ।. , 11'. j >.., ।118 I > .1iTr . 11.., 1111 11 (1111111 ।, Hp m/z 96.10 17.06% n/z—> 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 200 Abundance #102588:4-METHOXY-.BETA.-METHYLCINNAMIC ACID $$ 2-Butenoi... 192

108 . ............ I\ ......... 5000 22.00 22.20 22.40 22.60 146 175 m/z 191.10 16.28%

m/z—> 0 i ■' ■' i • ■ ■ ■ i"' ■ i ■' ‘' i' ■ ■' i • ‘■ i i ■ ■ • ■ i" ■ ■ i' ‘ ■ i 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 200 । ■ ■■1111 । ■ l unet Abundance #103424:3-Cyanocarbazole $$ 9H-Carbazole-3-carbonitriIe (CAS 192 —...................

22.00 22.20 22.40 22.60 5000 m/z 193.10 14.74%

96 164

miz—> ,.......... 01 1' i' ■' ■ i “' ‘ i ■''' i" ■ ■ i ■'" i' ■ 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 200 Ll 111 •'

Abundance #103936: Phenanthrene, 9-methyl- SS 9-Methylphenanthrene . i । , I | i'r b-r | i . , . । 1 I 192 22.00 22.20 22.40 22.60 m/z 146.10 14.34%

5000

96 165

m/z—> 88 J 01 T’B—0um—nmmmmtmnmnmnpn*WTp—ghgt 1 139 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 200 152 J 176 , A 22.00 22.20 22.40 22.60

)0165.D SCAN508.M Tue Feb 05 09:47:35 2002 Page 13

NYC-WTC_000050680

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NYC-WTC_000050680Source: NYC Law Department, mirrored locally

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