DEP GCMS data table, Jan-Feb 2002

Machine-extracted title · confidence 90%

Multi-page laboratory data sheet containing sample analysis results and metadata for DEP GCMS records from January to February 2002.

NYC-WTC_000004494–000004704

Folder label: “GCMS X 1/30/02 A 2/26/02”

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NYC 9/11 Public Portal Document Library Search Compound Report

Data File : C:\MSDCHEM\1\5973N\02FEB26\02088.D Vial: 5 Acq On : 26 Feb 2002 6:06 pm Operator: Sample : 508 scan Inst : Instrumen Mise : February 26, 2002 Multiplr: 1.00 MS Integration Params: LSCINT.P Quant Method : C:\MSDCHEM\1...\HP022102.M (RTE Integrator) Title : 508 scan method Library : C:\DATABASE\WILEY7N.L ********************************************************************* Peak Number 12 4-METHOXY-.BETA.-METHYLCINN... Concentration Rank 4

R.T. EstConc Area Relative to ISTD R.T.

22.28 0.11 ug/L 86074 Phenanthrene-dl0 22.63

Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 4-METHOXY-.BETA.-METHYLCINNAMIC ... 192 C11H1203 019169-94-9 72 2 3-Cyanocarbazole $$ 9H-Carbazole... 192 C13H8N2 057102-93-9 64 3 N-perdeuteriobenzylideneaniline 192 C13D11N 000538-51-2 64 4 Phenanthrene, 2-methyl- 192 C15H12 002531-84-2 53 Abundance Scan 1675 (22.283 min): 02088.D (-) m/z 192.00 100.00% 1'12

5000

... i.. M, 82 96 146 160 22.00 22.20 22.40 22.60 44 66 | 118 |, 0 . 11. ।(i।t r. । hanni...... r| — ।«1 • > ।»»• • । «1 > t •»i > i»»»> 111 i. (H r ,-j. • j * । m/ z 96.10 15.55% m/z-> 20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 200 Abundance #102588: 4-METHOXY-.BETA.-METHYLCINNAMIC ACID $$ 2-Butenoi... 192

108 5000 22.00 22.20 22.40 22.60 146 175 m/z 191.00 15.52%

0 " i " ■ ■ i " ' ■ i " 1111 ■ " i' " ‘ r " ■ r ■ " i " i " " i11" i" " i ■' ' i11 ri i" " i1 11111111 1TI m/z—> 20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 200 Abundance #103424: 3-Cyanocarbazole $$ 9H-Carbazole-3-carbonitrile (CAS 192 , .......... M...........M 22.00 22.20 22.40 22.60 5000 m/ z 193.10 14.80%

96 164 138 m/z-> 0 ' 11" ' 111 " I 20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 200 m r " ‘ i' 111 ■ ■ ■ ■ i • ■ ■ ■ I TT

Abundance #88409: N-perdeuteriobenzylideneaniline 192 22.00 22.20 22.40 22.60 m/z 146.00 14.18%

5000 82

54 110 30 94 160 0 ""I.. .. " i ■'1 ■ r " ■ i '' ।' 111111' Tmn mmT ------- m/z— > 20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 200 22.00 22.20 22.40 22.60

02088.D HP022102.M Wed Feb 27 08:35:16 2002 Page 14

NYC-WTC_000004642

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DEP GCMS data table, Jan-Feb 2002 · Box DEP Box 12

NYC-WTC_000004935

Multi-page laboratory data sheet containing sample analysis results and metadata for DEP GCMS records from January to February 2002.

3 shared non-person entities · 1 shared topics · Same agency, volume and box · similarity 0.999