Laboratory report listing unknown compounds and surrogate recovery for sample AE00105 analyzed on February 7, 2002.
NYC-WTC_000050793–000050812Folder label: “GCMS X 1/4/02 A 1/25/02”
OCR status: ok · source: pdftotext
NYC 9/11 Public Portal Document Library Search Compound Report Data File : C:\MSDCHEM\1\5973N\02JAN25\00105.D Vial: 3 Acq On : 25 Jan 2002 11:49 am Operator: Sample : 508 scan Inst : Instrumen Mise : January 25, 2002 Multiplr: 1.00 MS Integration Params: LSCINT.P Quant Method : C:\MSDCHEM\1...\SCAN508.M (RTE Integrator) Title : 508 scan method Library : C:\DATABASE\WILEY7N.L ********************************************************************* Peak Number 12 4-METHOXY-.BETA.-METHYLCINN... Concentration Rank 8
R.T. EstConc Area Relative to ISTD R.T.
22.28 0.15 ug/L 107342 Phenanthrene-dl0 22.65 Hit# of 5 Tentative ID MW MolForm CAS# Qual
1 4-METHOXY-.BETA.-METHYLCINNAMIC ... 192 C11H1203 019169-94-9 72 2 3-Cyanocarbazole $$ 9H-Carbazole... 192 C13H8N2 057102-93-9 64 3 N-perdeuteriobenzylideneaniline 192 C13D11N 000538-51-2 59 4 2-CYANOCARBAZOLE $$ 9H-Carbazole... 192 C13H8N2 057955-18-7 50 Abundance Scan 1656 (22.280 min): 00105. D (-) m/z 192.10 100.00% 192
5000 k i ■ ■ ■ ■ i 82 96 146 160 2200 22 20 22.40 22.60
m/z-> 44 ■ r ■ ...... I.... I.,. 118 ' 11"1111" I — 20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 200 ll. m/z 193.10 17.55% Abundance #102588:4-METHOXY-.BETA.-METHYLCINNAMIC ACID $$ 2-Butenoi... 192
108 5000 T T T 22 00 22.20 22.40 22.60 146 175 m/z 191.10 16.36%
I'’ r ■ ■ ■ i "r' i" J' r ■ " i" " i T‘" T1"1111 " " I " " I " Ii.. TTIT m/z-> 20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 200 Abundance #103424: 3-Cyanocarbazole $$ 9H-Carbazole-3-carbonrtrile (CAS 192
22 00 22.20 22.40 22.60 5000 m/ Z 96.00 15.92%
96 164
n/z-> c TTTTTTT 138 r" 1’1 Tr 20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 200 I II Abundance #88409: N-perdeuteriobenzylideneaniline 192 22.00 22.20 22.40 22.60 m/z 146.10 13.87%
5000 82
54 110 30 1 94 160 A ) Th I " '' I I" '' I । II ■■■nil. f. " r' " r ' " r ■'' i' ■" I" ■ ■ r "' r'' । ' ■ • ' r T 1
m/z-> 20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 200 22.00 22.20 22.40 22.60
00105.D SCAN508.M Mon Jan 28 09:49:49 2002 Page 14
NYC-WTC_000050810
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NYC-WTC_000051364
Laboratory report showing GCMS analysis of sample AE00314 with surrogate recovery data on January 24, 2002.
1 shared non-person entities · 1 shared topics · Same agency, volume and box · similarity 0.997
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000051236
Laboratory report documenting gas chromatography-mass spectrometry analysis of environmental sample AE00366 conducted on January 18, 2002.
1 shared non-person entities · 1 shared topics · Same agency, volume and box · similarity 0.996
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000051642
Laboratory report showing GCMS analysis results for sample AE00616 conducted on February 1, 2002.
1 shared non-person entities · 1 shared topics · Same agency, volume and box · similarity 0.996
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000051567
Laboratory report showing GCMS analysis results for sample AE00562 conducted on February 1, 2002.
1 shared non-person entities · 1 shared topics · Same agency, volume and box · similarity 0.996
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000051422
Laboratory report showing GCMS analysis of sample AE00463 with surrogate recovery data on January 24, 2002.
1 shared topics · Same agency, volume and box · similarity 0.996
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000051055
Laboratory report showing GCMS analysis of sample AE00307 for unknown compounds and DDD on January 10, 2002.
1 shared non-person entities · 1 shared topics · Same agency, volume and box · similarity 0.996
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000051301
Laboratory report showing GCMS analysis of sample AE00471 with surrogate recovery data on January 18, 2002.
1 shared non-person entities · 1 shared topics · Same agency, volume and box · similarity 0.996
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000050664
Laboratory report listing unknown compounds and surrogate recovery for sample AE00165 analyzed on February 13, 2002.
1 shared topics · Same agency, volume and box · similarity 0.996
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000037720
Laboratory report documenting GCMS analysis of a method blank for sample AE03612 to verify analytical system cleanliness.
1 shared topics · similarity 0.996
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000010967
Gas chromatography-mass spectrometry analysis of sample AE02718 performed March 5, 2002, documenting other unknown compounds and surrogate 2,4-DDD recovery at 97 percent.
1 shared topics · similarity 0.995
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000037780
Gas chromatography-mass spectrometry analysis of sample AE03616 performed on 3/28/2002, detecting other unknown compounds with surrogate 2,4-DDD at 5.0 µg detection limit.
1 shared topics · similarity 0.995
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000004494
Multi-page laboratory data sheet containing sample analysis results and metadata for DEP GCMS records from January to February 2002.
1 shared non-person entities · 1 shared topics · similarity 0.995
machine-extracted · confidence unavailable · Check page ↗Similar subjects in other documents. Similarity does not establish the same event, measurement or conclusion.
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NYC-WTC_000050702
Administrative record from DEP Box 28 documenting CCMS activities at the World Trade Center site in January 2002.
Filed in the same folder
NYC-WTC_000050703
Technical log recording method parameters and sample processing details for a DEP laboratory procedure between January 4 and 25, 2002.
Filed in the same folder
NYC-WTC_000050705
Laboratory report listing concentrations of volatile organic compounds in sample AE00027 analyzed on January 25, 2002.
Filed in the same folder
NYC-WTC_000050709
Reference standard GCMS analysis for sample AE00027 performed on January 25, 2002, providing quality control results.
Filed in the same folder
NYC-WTC_000050716
Laboratory report showing non-detect results for volatile organic compounds in a GCMS blank analyzed on January 25-February 7, 2002.
Filed in the same folder