GCMS analysis results for sample AE01637, March 2002

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GCMS laboratory results for sample AE01637 conducted on March 5, 2002, showing surrogate recovery and unknown compounds.

NYC-WTC_000010106–000010125

Folder label: “GCMS X 1/23/02 A 2/21/02”

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NYC 9/11 Public Portal Document

Library Search Compound Report Data File : C:\MSDCHEM\l\5973N\02FEB21\01637.D Vial: 6 Acq On : 21 Feb 2002 7:22 pm Operator: Sample : 508 scan Inst : Instrumen Mise : February 21, 2002 Multiplr: 1.00 MS Integration Params: LSCINT.P Quant Method : C:\MSDCHEM\1. . .\HP022102.M (RTE Integrator) Title : 508 scan method Library : C:\DATABASE\WILEY7N.L ********************************************************************* Peak Number 12 4-METHOXY-.BETA.-METHYLCINN... Concentration Rank 4 R.T. EstConc Area Relative to ISTD R.T. 22.28 0.12 ug/L 85657 Phenanthrene- dl 0 22.63 Hit# of 5 Tentative ID MW MolForm CAS# Qual 1 4-METHOXY-.BETA.-METHYLCINNAMIC ... 192 C11H1203 019169-94-9 64 2 3-Cyanocarbazole $$ 9H-Carbazole... 192 C13H8N2 057102-93-9 64 3 Phenanthrene, 9-methyl- $$ 9-Met... 192 C15H12 000883-20-5 59 4 N-perdeuteriobenzylideneaniline 192 C13D11N 000538-51-2 52 Abundance Scan 1675 (22.283 min): 01637.D (-) m/z 192.00 100.00% 192

5000

96 ■ ■ i ■ ‘ Trfr 82 146 160 22.00 22.20 22.40 2260

miz—> 49 118 1. pummmmPm 0 I M > *‘i * 1 * 1 j • * > ■ । i TTI— । i TT-p-rrrp- 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 200 II——— m/z 96.00 17.40% Abundance #102588:4-METHOXY-BETA.-METHYLCINNAMIC ACID $$ 2-Butenoi... 1$2

108 5000 T 188 22.00 22.20 22.40 22.60 146 175 m/z 146.10 15.52%

n/z—> 0- i “ " i‘ ■ i■ ■1 ■ i11' ■ i■ ■" i" “ i • ■

Abundance 1111111*441’1*118* 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 200 ■ i ■" ■ i ■ “ ■ i ■

#103424: 3-Cyanocarbazole $$ 9H-Carbazole-3-carbonitrile (CAS 1 ■ i" " i1 u 192 .......A..... L 22.00 22.20 22.40 22.60 5000 m/z 193.10 14.78%

96 164

m/z—> 01 “ ■ ■ i ■ ‘" i ■ ■ ■ ■ i" ■11"' ■ i “

40 50 60 mIT 138

70 80 90 1(M 110 120 130 140 150 160 170 180 190 200 l TTI-

Abundance #103936: Phenanthrene, 9-methyl- $$ 9-Methylphenanthrene 192 22.00 22.20 22.40 22.60 m/z 191.00 14.16% 5000

m/z—> 96 88 l 139 152 165 0-1-3191-92000 —1—023 — TTT Wt-t 176 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 200 TI T 22.00 22.20 22.40 22.60 A 01637.D HP022102.M Mon Feb 25 10:55:45 2002 Page 14

NYC-WTC_000010123

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GCMS analysis report for sample AE01636, March 2002 · Box DEP Box 14

NYC-WTC_000010086

GCMS laboratory results for sample AE01636 conducted on March 5, 2002, showing surrogate recovery and unknown compounds.

1 shared non-person entities · 1 shared topics · Same agency, volume and box · similarity 0.998