DEP GCMS data table, Jan-Feb 2002

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Multi-page laboratory data sheet containing sample analysis results and metadata for DEP GCMS records from January to February 2002.

NYC-WTC_000004935–000005145

Folder label: “GCMS X 2/1/02 A 2/27/02”

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NYC 9/11 Public Portal Document Library Search Compound Report

Data File : C: \MSDCHEM\1\5973N\02FEB27\02385.D Vial: 1 Acq On : 27 Feb 2002 3:17 pm Operator: Sample : 508 scan Inst : Instrumen Mise : February 27, 2002 Multiplr: 1.00 MS Integration Params: LSCINT.P

Quant Method : C:\MSDCHEM\l-..\HP022102.M (RTE Integrator) Title : 508 scan method Library : C:\DATABASE\WILEY7N.L ********************************************************************* Peak Number 12 4-METHOXY-.BETA.-METHYLCINN... Concentration Rank 5

R.T. EstConc Area Relative to ISTD R.T.

22.28 0.12 ug/L 89212 Phenanthrene-dl0 22.64

Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 4-METHOXY-.BETA.-METHYLCINNAMIC ... 192 C11H1203 019169-94-9 72 2 2,4-Diamino-6-(hydroxymethyl)pte... 192 C7H8N6O 000945-24-4 64 3 3-Cyanocarbazole $$ 9H-Carbazole... 192 C13H8N2 057102-93-9 64 4 N-perdeuteriobenzylideneaniline 192 C13D11N 000538-51-2 58 Abundance Scan 1675 (22.283 min): 02385.D (-) m/z 192.00 100.00% 192

5000

82 96 146 160 m 22.00 22.20 22.40 22.60 44 70 —— Of pTTIIT TP "J... I ।1 ■1 ■ ।111' ।' ■ ■' ।"11 ■1 ’IT TP m/z 14 6.00 16.42% m/z-> 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 200 Abundance #102588: 4-METHOXY-.BETA.-METHYLCINNAMIC ACID $$ 2-Butenoi... 102

5000 108 ...... A..... IL 22.00 22,20 22.40 22.60 146 175 m/z 96.00 15.80%

m/z-> 0 1′1211:1/1/1112111111011137 ।"1 ■ i1" ■ ।'11 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 200 11" " i " " r u Abundance #102010:2,4-Diamino-6-(hydroxymethyl)pteridine 192 163 22.00 22.20 22.40 22.60 5000- m/ Z 191.10 13.49%

66 146 175 121 135 0 34 r 111 r ' “ i " " i I ' i " '' i " " i " " I' ‘ " i " " i " " i1 . ........ II..,,I,.. .. ....... 1 ■ i111111 m/z-> 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 200 Abundance #103424: 3-Cyanocarbazole $$ 9H-CarbazoIe-3-carbonitrile (CAS 192 22.00 22.20 22.40 22.60 m/z 193.00 13.24%

5000

96 164 138 0 r ■ " i'''' i I"1■ I i" " i 1’01111101710111111111111’111- 1' I " " 11 " 1 r TIT m/z-> 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 200 22.00 22.20 22.40 22.60

02385.D HP022102.M Thu Feb 28 08:47:04 2002 Page 14

NYC-WTC_000005023

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DEP GCMS data table, Jan-Feb 2002 · Box DEP Box 12

NYC-WTC_000004494

Multi-page laboratory data sheet containing sample analysis results and metadata for DEP GCMS records from January to February 2002.

3 shared non-person entities · 1 shared topics · Same agency, volume and box · similarity 0.999