Laboratory report listing unknown compounds and surrogate recovery for sample AE00249 analyzed on January 28, 2002.
NYC-WTC_000050577–000050595Folder label: “GCMS X 1/4/02 A 1/24 - 1/25/02”
OCR status: ok · source: pdftotext
NYC 9/11 Public Portal Document Library Search Compound Report
Data File : C:\MSDCHEM\1\5973N\02JAN24\00249.D Vial: 5 Acq On : 24 Jan 2002 6:17 pm Operator: Sample : 508scan Inst : Instrumen Mise : January 24, 2002 Multiplr: 1.00 MS Integration Params: LSCINT.P Quant Method : C:\MSDCHEM\1...\SCAN508.M (RTE Integrator) Title : 508 scan method Library- : C:\DATABASE\WILEY7N.L ********************************************************************* Peak Number 5 4-METHOXY-.BETA.-METHYLCINN... Concentration Rank 10 R.T. EstConc Area Relative to ISTD R.T. 22.28 0.14 ug/L 103730 Phenanthrene-dl0 22.65
Hit# of 5 Tentative ID MW Mol Form CAS# Qual
1 4-METHOXY-.BETA.-METHYLCINNAMIC ... 192 C11H1203 019169-94-9 72 2 3-Cyanocarbazole $$ 9H-Carbazole. .. 192 C13H8N2 057102-93-9 59 3 2,4-Diamino-6-(hydroxymethyl)pte. .. 192 C7H8N60 000945-24-4 53 4 1,3-Benzodioxole, 4-methoxy-6-(2... 192 C11H12O3 000607-91-0 52 Abundance Scan 1656 (22.280 min): 00249.D (-) m/z 192.10 100.00% 1912
5000 ............. / ............. , 82 96 146 160 22.00 22.20 22.40 22.60 miz-> 42 52 —pmmmmmm70 | 118 ' i"' 11 ■. ■' i ■'' ■ i ■ 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 200 Al m/ z 146.10 16.49% Abundance #102588:4-METHOXY-BETA.-METHYLCINNAMIC ACID $$ 2-Butenoi... 102
5000 108 . A......... { A ■ r "22.60 22.20 22.40 22.60 ‘ 146 175 m/z 96.00 14.57%
n/z-> U ■ ■ i ■ ■ ■ ■ i ■ ■ “ I"' ■ i ■' ‘ • I'11 ■ I'1 ■ ■ i “ ■ ■ i" ■ 1’—’1—0T3T7T1"237 ■ i'1 ■ ■ i ■ ■ ■ ■ i ■ HP 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 200 Abundance #103424:3-Cyanocarbazole $$ 9H-Carbazole-3-carbonitrile (CAS 192
'22.00 22.20 22.4a 2200 5000 m/z 191.00 14.22%
96 164 l 138 mmmmpmmmmmmmmmmmmmmmmpmpp Ila. miz-> 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 200 Abundance #102010:2,4-Diamino-6-(hydroxymethyl)pteridine 15 2 22.00 22.20 22.^) 22.60 163 m/z 193.10 13.91%
5000
66 146 121 135 ll..... 34 ’I1’01T1003U1’T ' i'''‘i" "i" "i"" i"'‘i"" i"" i‘ Mh । * “ । ■1 1 ■ i ' ■ ' ■ i '' ■ ■ i ' ■ • ‘ i ’ 1
m/z—> 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 200 22.00 22.20 22.40 22.60
00249.D SCAN508.M Fri Jan 25 10:26:17 2002 Page 7
NYC-WTC_000050587
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NYC-WTC_000051605
Laboratory report showing GCMS analysis results for sample AE00614 conducted on February 1, 2002.
1 shared non-person entities · 1 shared topics · Same agency, volume and box · similarity 0.997
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000049957
Laboratory report showing GCMS analysis of sample AD31639 including unknown compounds and surrogate recovery data.
1 shared non-person entities · 1 shared topics · Same agency, volume and box · similarity 0.997
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000052147
Laboratory report showing GCMS analysis of sample AE00832 including surrogate recovery and unknown compounds.
1 shared topics · Same agency, volume and box · similarity 0.996
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000052088
Laboratory report showing GCMS analysis of sample AE00839 including surrogate recovery and unknown compounds.
1 shared topics · Same agency, volume and box · similarity 0.996
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000052128
Laboratory report showing GCMS analysis of sample AE00843 including surrogate recovery and unknown compounds.
1 shared topics · Same agency, volume and box · similarity 0.996
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000050205
Laboratory report documenting GCMS analysis of sample AD31647 with detection of unknown compounds and surrogate recovery.
1 shared topics · Same agency, volume and box · similarity 0.996
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000050558
Laboratory report listing unknown compounds and surrogate recovery for sample AE00248 analyzed on January 28, 2002.
1 shared topics · Same agency, volume and box · similarity 0.996
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000050500
Laboratory report for sample AE00168 documenting detection of unknown compounds and surrogate recovery on January 28, 2002.
1 shared topics · Same agency, volume and box · similarity 0.995
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000009946
Analytical results for sample AE01507 analyzed via GCMS on March 4, 2002, including surrogate recovery data.
1 shared topics · similarity 0.996
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000010027
GCMS laboratory results for sample AE01510 conducted on March 5, 2002, showing surrogate recovery and unknown compounds.
1 shared non-person entities · 1 shared topics · similarity 0.995
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000037680
Laboratory report documenting GCMS analysis of a method blank for sample AE03510 to verify analytical system cleanliness.
1 shared non-person entities · 1 shared topics · similarity 0.995
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000009966
Analytical results for sample AE01508 analyzed via GCMS on March 4, 2002, including surrogate recovery data.
1 shared non-person entities · 1 shared topics · similarity 0.995
machine-extracted · confidence unavailable · Check page ↗Similar subjects in other documents. Similarity does not establish the same event, measurement or conclusion.
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NYC-WTC_000050432
Administrative record from DEP Box 28 documenting GCMS activities at the World Trade Center site in January 2002.
Filed in the same folder
NYC-WTC_000050433
Fragmented page containing a document identifier and instructions regarding liquid-liquid extractor drip rates from January 24-25, 2002.
Filed in the same folder
NYC-WTC_000050435
Gas chromatography-mass spectrometry calibration analysis of sample AE00167 detecting multiple organic compounds including nitrosamines and dichlorobenzenes.
Filed in the same folder
NYC-WTC_000050439
Laboratory report listing concentrations of volatile organic compounds in sample AE00167 analyzed on January 24-25, 2002.
Filed in the same folder
NYC-WTC_000050444
Laboratory blank report for GCMS analysis of sample AE00167 showing compound concentrations and quality control values.
Filed in the same folder