Laboratory report listing unknown compounds and surrogate recovery for sample AE00249 analyzed on January 28, 2002.
NYC-WTC_000050577–000050595Folder label: “GCMS X 1/4/02 A 1/24 - 1/25/02”
OCR status: ok · source: pdftotext
NYC 9/11 Public Portal Document Library Search Compound Report . Data File : C:\MSDCHEM\1\5973N\02JAN24\00249.D Vial: 5 Acq Ori : 24 Jan 2002 6:17 pm Operator: Sample : 508scan Inst : Instrumen Mise : January 24, 2002 Multiplr: 1.00 MS Integration Params: LSCINT.P Quant Method : C:\MSDCHEM\1. . .\SCAN50 8. M (RTE Integrator) Title : 508 scan method Library : C:\DATABASE\WILEY7N.L ********************************************************************* Peak Number 4 3-(CYCLOHEX-3'-EN-YL)PROPAN... Concentration Rank 1
R.T. EstConc Area Relative to ISTD R.T.
5.89 4.39 ug/L 1887100 1, 4-Dichlorobenzene-d4 9.72
Hit# of 5 Tentative ID MW MolForm CAS# Qual 1 3-(CYCLOHEX-3'-EN-YL)PROPANOL $$... 174 C8H1404 015745-87-6 33 2 Acetic acid, 3-[1,3]dioxolan-2-y... 174 C8H14O4 000000-00-0 33 3 N-Ethylformamide $$ N-Formylethy. . . 73 C3H7NO 000627-45-2 9 4 3-Pentanol, 3-methyl- (CAS) $$ 3... 102 C6H140 000077-74-7 9 Abundance Scan 220 (5.885 min): 00249.0 (-) m/z 73.10 100.00%
L 73
5000 43 5.60 5.80 6.00 6.20 . r. .. . .. .1 1 55 ■■4.............. m/z 43.10 24.51% niz-> 10 20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 Abundance #36138:3-(CYCLOHEX-3'-EN-YL)PROPANOL $$ 2-Cyclohexene-1-p... 73
5000 5.60 5.80 6.00 6.20 43 m/z 41.10 9.35% 27 55 87 113 174 TIPgtr11-1111111193 1 +p । . : . i । . . t i j . . . . । » » » i j . t > i । . i ii fTi । i J i » . I | • । । i | • miz-> 10 20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 Abundance #78238: Acetic acid, 3-[1,3]dioxolan-2-ylpropyl ester 73 5.60 A 5.80 6.00 6.20 5000 m/z 45.10 9.32% 43 27 87 Tppp ‘ I “55" I " “ I1‘ Hpenj... a|....113 t...i(।11।।11 174 nfa-> 10 20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 Abundance #1794: N-Ethylformamide $$ N-Formylethylamine $$ Formamide... 30 5.60 5.80 6.00 6.20 73 m/z 71.10 6.89% 5000- 44 58
m/z—> m 15 Apr I************ 10 20 30 40 50 60 70 80 90 1(X) 110 120 130 140 150 160 170 180 . A, 5.60 5.80 6.00 6.20
00249.D SCAN508.M Fri Jan 25 10:26:17 2002 Page 6
NYC-WTC_000050586
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NYC-WTC_000051605
Laboratory report showing GCMS analysis results for sample AE00614 conducted on February 1, 2002.
1 shared non-person entities · 1 shared topics · Same agency, volume and box · similarity 0.997
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000049957
Laboratory report showing GCMS analysis of sample AD31639 including unknown compounds and surrogate recovery data.
1 shared non-person entities · 1 shared topics · Same agency, volume and box · similarity 0.997
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000052147
Laboratory report showing GCMS analysis of sample AE00832 including surrogate recovery and unknown compounds.
1 shared topics · Same agency, volume and box · similarity 0.996
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000052088
Laboratory report showing GCMS analysis of sample AE00839 including surrogate recovery and unknown compounds.
1 shared topics · Same agency, volume and box · similarity 0.996
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000052128
Laboratory report showing GCMS analysis of sample AE00843 including surrogate recovery and unknown compounds.
1 shared topics · Same agency, volume and box · similarity 0.996
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000050205
Laboratory report documenting GCMS analysis of sample AD31647 with detection of unknown compounds and surrogate recovery.
1 shared topics · Same agency, volume and box · similarity 0.996
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000050558
Laboratory report listing unknown compounds and surrogate recovery for sample AE00248 analyzed on January 28, 2002.
1 shared topics · Same agency, volume and box · similarity 0.996
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000050500
Laboratory report for sample AE00168 documenting detection of unknown compounds and surrogate recovery on January 28, 2002.
1 shared topics · Same agency, volume and box · similarity 0.995
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000009946
Analytical results for sample AE01507 analyzed via GCMS on March 4, 2002, including surrogate recovery data.
1 shared topics · similarity 0.996
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000010027
GCMS laboratory results for sample AE01510 conducted on March 5, 2002, showing surrogate recovery and unknown compounds.
1 shared non-person entities · 1 shared topics · similarity 0.995
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000037680
Laboratory report documenting GCMS analysis of a method blank for sample AE03510 to verify analytical system cleanliness.
1 shared non-person entities · 1 shared topics · similarity 0.995
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000009966
Analytical results for sample AE01508 analyzed via GCMS on March 4, 2002, including surrogate recovery data.
1 shared non-person entities · 1 shared topics · similarity 0.995
machine-extracted · confidence unavailable · Check page ↗Similar subjects in other documents. Similarity does not establish the same event, measurement or conclusion.
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NYC-WTC_000050432
Administrative record from DEP Box 28 documenting GCMS activities at the World Trade Center site in January 2002.
Filed in the same folder
NYC-WTC_000050433
Fragmented page containing a document identifier and instructions regarding liquid-liquid extractor drip rates from January 24-25, 2002.
Filed in the same folder
NYC-WTC_000050435
Gas chromatography-mass spectrometry calibration analysis of sample AE00167 detecting multiple organic compounds including nitrosamines and dichlorobenzenes.
Filed in the same folder
NYC-WTC_000050439
Laboratory report listing concentrations of volatile organic compounds in sample AE00167 analyzed on January 24-25, 2002.
Filed in the same folder
NYC-WTC_000050444
Laboratory blank report for GCMS analysis of sample AE00167 showing compound concentrations and quality control values.
Filed in the same folder