GCMS analysis report for sample AE01507, March 2002

NYC 9/11 Public Portal Document

Library Search Compound Report . Data File : C:\MSDCHEM\1\5973N\02FEB21\01508.D Vial: 8 Acq On : 21 Feb 2002 9:01 pm Operator: Sample : 508 scan fb Inst : Instrumen Mise : February 21, 2002 Multiplr: 1.00 MS Integration Params: LSCINT.P Quant Method : C:\MSDCHEM\1...\HP022102 .M (RTE Integrator) Title : 508 scan method Library : C:\DATABASE\WILEY7N.L ********************************************************************* Peak Number 7 3-(CYCLOHEX-3'-EN-YL)PROPAN... Concentration Rank 2 R.T. EstConc Area Relative to ISTD R.T. 5.95 0.38 ug/L 177120 1,4-Dichlorobenzene-d4 9.72 Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 3-(CYCLOHEX-3'-EN-YL)PROPANOL $$... 174 C8H14O4 015745-87-6 33 2 Acetic acid, 3-[1,3]dioxolan-2-y... 174 C8H14O4 000000-00-0 33 3 N-Ethylformamide $$ N-Formylethy... 73 C3H7NO 000627-45-2 9 4 1-Hexanamine 101 C6H15N 000111-26-2 9 Abundance Scan 228 (5.948 min): 01508.D (-) m/z 73.10 100.00% 73

5000

43 1 ■ i • 1 • ■ i ■ ■ ■ ■ i ■ ■ ■ • i ■ ■ ‘ 1 l 1 5.60 5.80 6.00 6.20 —nP 55 H 87 103 0" 11111 j > 11: । > TneagnmmpTng m/z 43.10 . 20.90% miz-> 10 20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 Abundance #36138:3-(CYCLOHEX-3'-EN-YL)PROPANOL $$ 2-Cyclohexene-1-p... 73

5000 TT——mprP ■ ■ । — 5.60 5.806.00 6.20 43 m/ z 45.10 10.12% 27 55 , 87 113 174 0- ■ ■ i ■■ ■ • i “ “ i • ■ Tp HpI************************* miz—> 10 20 30 40 50 60 70 80 90 1(X) 110 120 130 140 150 160 170 180 Abundance #78238: Acetic acid, 3-[1,3]dioxolan-2-ylpropyl ester 73 MM....... , 5.60 5.80 6.00 6.20 1,1 5000 m/z 41.10 . 8.83% 43 27 55...... ■■ 1, —m1—001100010 87 113 174 0- Tptr —011—0—0——m——mTn miz-> 10 20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 Abundance #1794: N-Ethylformamide $$ N-Formylethylamine $$ Formamide... • • i 1 ■ ■ ■ i 1 30 5.60 5.80 6.00 6.20 73 m/z 71.10 6.53% 5000 44 58

15

m/z—> 0-m10pul. TTTTTTTTTTTITTTWTTTLTTTTTWTTIWTTTITTTTT 20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 ■ ■ i ■ • ■ ■ । 1 ■ ■ ■ t ’ • 1 ■ i ■ ‘ 1 ■ i • 5.60 5.80 6.00 6.20

01508.D HP022102.M Mon Feb 25 10:54:57 2002 Page 9

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