DEP GCMS data table, Jan-Feb 2002

NYC 9/11 Public Portal Document Library Search Compound Report

Data File : C:\MSDCHEM\1\5973N\02FEB27\02387.D Vial: 3 Acq On : 27 Feb 2002 4:57 pm Operator: Sample : 508 scan Inst : Instrumen Mise : February 27, 2002 Multiplr: 1.00 MS Integration Params: LSCINT.P Quant Method : C:\MSDCHEM\1...\HP022102.M (RTE Integrator) Title : 508 scan method Library : C:\DATABASE\WILEY7N. L ********************************************************************* Peak Number 5 3-(CYCLOHEX-3'-EN-YL)PROPAN... Concentration Rank 2 R.T. EstConc Area Relative to ISTD R.T. 5.94 0.39 ug/L 170482 1,4-Dichlorobenzene-d4 9.72 Hit# of 5 Tentative ID MW MolForm CAS# Qual 1 3-(CYCLOHEX-3'-EN-YL)PROPANOL $$... 174 C8H14O4 015745-87-6 37 2 Acetic acid, 3-[1,3]dioxolan-2-y... 174 C8H14O4 000000-00-0 37 3 N-Ethylformamide $$ N-Formylethy... 73 C3H7NO 000627-45-2 9 4 1,3-Dioxolane, 2-pentadecyl- $$ ... 284 C18H36O2 004360-57-0 9 Abundance Scan 227 (5.936 min): 02387. D (-) m/z 73.10 100.00% 73

5000 43 ................... ... ■ 1 1 ■ । 1 । 111 1 ■ ' ' i 5.60 5.80 6.00 6.20 , 86 0-- 1111111111111 TEUD 103 —PPmg 55... ,1 m/z 43.10 27.96% miz-> 10 20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 Abundance #36138: 3-(CYCLOHEX-3'-EN-YL)PROPANOL $$ 2-Cyclohexene-1-p... 73

5000 5.60 5.80 6.00 6.20 43 m/z 45.10 9.24% 27 55 , 87 113 174 0- " i " " i " " r T4r 11100-117111, I 1 " I mTToni I " '' I fTi 11 IFutpuTp , k. 11 i >, I., 11JI»1111 m/z-> 10 20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 Abundance #78238: Acetic acid, 3-[1,3]dioxolan-2-ylpropyl ester 73 * ■ । 1 1 1 * i ' ‘ 1 i 5.60 5.80 6.00 6.20 5000 m/ z 41.10 8.84%

43 27 55 87 113 174 0- ' ■ r ' " i' " ‘ i' TT4 11" " i " ' ’, i'i Tp TNOuumuum)ITTI]" m/z-> 10 20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 Abundance #1794: N-Ethylformamide $$ N-Formylethylamine $$ Formamide... 30 1 ...... 5.60 5.80 6.00 6.20 73 m/z 71.00 7.54%

5000 44 58

15

m/z-> 0 H — 1 " " i'11'11 " '' i ■ " ■ I " ■' i ■ " ■ i'1'' i1 ■ ■' i'' " i1 " ' i11 " i1 " 11' 10 20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 5.60 5.80 ,1,,,,,,,,,,, , 6.00 6.20

32387.D HP022102.M Thu Feb 28 08:47:16 2002 Page 7

NYC-WTC_000005056