DEP GCMS data table, Jan-Feb 2002

Machine-extracted title · confidence 90%

Multi-page laboratory data sheet containing sample analysis results and metadata for DEP GCMS records from January to February 2002.

NYC-WTC_000004494–000004704

Folder label: “GCMS X 1/30/02 A 2/26/02”

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NYC 9/11 Public Portal Document Library Search Compound Report Data File : C:\MSDCHEM\1\5973N\02FEB26\02089.D Vial: 6 Acq On : 26 Feb 2002 6:55 pm Operator: Sample : 508 scan Inst : Instrumen Mise : February 2 6, 2002 Multiplr: 1.00 MS Integration Params: LSCINT.P Quant Method : C:\MSDCHEM\l-..\HP022102.M (RTE Integrator) Title : 508 scan method Library : C:\DATABASE\WILEY7N.L ********************************************************************* Peak Number 6 3 -(CYCLOHEX-3'-EN-YL)PROPAN. .. Concentration Rank 1 R.T. EstConc Area Relative to ISTD R.T. 5.94 0.48 ug/L 223121 1,4-Dichlorobenzene-d4 9.72 Hit# of 5 Tentative ID MW MolForm CAS# Qual

13-(CYCLOHEX-3'-EN-YL)PROPANOL $$... 174 C8H1404 015745-87-6 33 2 Silane, tetramethyl- $$ Tetramet... 88 C4H12Si 000075-76-3 33 3 Acetic acid, 3-[1,3]dioxolan-2-y... 174 C8H14O4 000000-00-0 33 4 N-Ethylformamide $$ N-Formylethy... 73 C3H7NO 000627-45-2 9 Abundance Scan 227 (5.936 min): 02089.D (-) m/ z 73.10 100.00% 73

5000

43 5.60 5.80 6.00 6.20 0- " I'I " 155... H TTn ! 87 103 ———OOgmmpuuonummOu ' '' I 11 '' I' 11 'I ' ' 1 'I1 m/z 43.10 23.63% m/z-> 10 20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 Abundance #36138:3-(CYCLOHEX-3’-EN-YL)PROPANOL $$ 2-Cyclohexene-1-p... 73

5000 — —PATAN 4 5.60 5.80 6.00 6.20 43 m/z 45.10 9.92% 27 55 , 87 113 174 0-TTOOg 11" " i " 11. 1I ' TeumduOumOTTETPuupr m/z-> 10 20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 Abundance #4812: Silane, tetramethyl- $$ Tetramethylsilane $$ (CH3)4... 73 5.60 5.80 6.00 '' 6.20 ' ' ' 5000 m/z 41.10 9.67%

45 15 31 , I |-i55 111 11 r 1 88 O-TTT । 1111111 1" i'"11"r ■ ।। ■1" ।"1' ।'11" " ।।1" ■ ।। ‘ m/z-> 10 20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 Abundance #78238: Acetic acid, 3-[1,3]dioxolan-2-ylpropyl ester 73 A.......... / -AA-AA 5.60 5.80 6.00 6.20 m/ z 71.10 6.35%

5000

43 27 87 55 113 , 174 0 ■ ■ i' ■ " i1' ■' i1 TT- 11" ■' i1 “ ’.I’i 1 " I " 1 ‘ i'1" 11" 1111" " I " 1' I " 111117 Trrt* 1"1111 . ] n/z—> 10 20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 5.60 5.80 6.00 6.20 .

02089.D HP022102.M Wed Feb 27 08:35:21 2002 Page 8

NYC-WTC_000004656

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NYC-WTC_000004656Source: NYC Law Department, mirrored locally

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DEP GCMS data table, Jan-Feb 2002 · Box DEP Box 12

NYC-WTC_000004935

Multi-page laboratory data sheet containing sample analysis results and metadata for DEP GCMS records from January to February 2002.

3 shared non-person entities · 1 shared topics · Same agency, volume and box · similarity 0.999