GCMS results for sample AE00321, Jan 24 2002

NYC 9/11 Public Portal Document

Library Search Compound Report Data File : C:\MSDCHEM\1\5973N\02JAN11\00321.D Vial: 2 Acq On : 11 Jan 2002 2:57 pm Operator: Sample : 508 scan Inst : Instrumen Mise : January 11, 2002 Multiplr: 1.00 MS Integration Params: LSCINT.P Quant Method : C:\MSDCHEM\l-..\SCAN508.M (RTE Integrator) Title : 508 scan method Library : C:\DATABASE\WILEY7N.L ********************************************************************* Peak Number 4 3-(CYCLOHEX-3'-EN-YL)PROPAN... Concentration Rank 1 R.T. EstConc Area Relative to ISTD R.T.

5.89 5.27 ug/L 1859510 1,4-Dichlorobenzene-d4 9.72

Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 3-(CYCLOHEX-3'-EN-YL)PROPANOL $$... 174 C8H14O4 015745-87-6 33 2 Acetic acid, 3-[1,3]dioxolan-2-y... 174 C8H14O4 000000-00-0 33 3 Silane, tetramethyl- $$ Tetramet... 88 C4H12Si 000075-76-3 28 4 N-Ethylformamide $$ N-Formylethy... 73 C3H7NO 000627-45-2 9 Abundance Scan 220 (5.886 min): 00321 .D (-) m/z 73.10 100.00% 73

5000

43

n/z-> 0 11'i1 55 TTTOTTuf+ 11 I । 87 103 i■ ■■■i ■i i ■1 ■ ■ i' ■ ■ ■ i1 ■ ■' i ■ 10 20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 m/z 5.60 5.80 43.10 6.00 6.20 23.94% Abundance #36138: 3-(CYCLOHEX-3'-EN-YL)PROPANOL $$ 2-Cyclohexene-1-p... 78

5000 5.60 5.80 6 00 6.20 43 m/z 45.10 9.11% 27 55 87 113 174 o1 11111 ■ i' ■ Tr Ttr 1 r ■ " r ■r ■ , iI 1 *9IT0]auan***unu—a—n]————uat m/z-> 10 20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 Abundance #78238: Acetic acid, 3-[1,3]dioxolan-2-ylpropyl ester 73 5.60 5.80 6.00 6.20 5000 m/z 41.10 8.92% 43 -.......... __ 27 55 87 113 174 0- 'I" "I"'1...... ’I’t" ■ r 1'11" 1 ’,I’I m/z-> 10 20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 Abundance #4812: Silane, tetramethyl- $$ Tetramethylsilane $$ (CH3)4... 78 5.60 5.80 6.00 6.20 m/z 71.10 6.51% 5000

45 15 31 | 55 01...... '.'I........ " ■ t1P" l ■ 1 88 ... . 1" । "11" " ।"1 ■ ।1" ■ ।।।...... ।।।. A... . m/z-> 10 20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 5.60 5.80 6.00 6.20

00321.D SCAN508.M Mon Jan 14 10:46:42 2002 Page 6

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