GCMS results for sample AE00321, Jan 24 2002

NYC 9/11 Public Portal Document

Library Search Compound Report Data File : C:\MSDCHEM\1\5973N\02JAN11\00321.D Vial: 2 Acq On : 11 Jan 2002 2:57 pm Operator: Sample : 508 scan Inst : Instrumen Mise : January 11, 2002 Multiplr: 1.00 MS Integration Params: LSCINT.P Quant Method : C:\MSDCHEM\1...\SCAN508 :M (RTE Integrator) Title : 508 scan method Library : C:\DATABASE\WILEY7N.L Peak Number 3 Butenol, methyl- Concentration Rank 3

R.T. EstConc Area Relative to ISTD R.T. 5.02 0.19 ug/L 65385 1,4-Dichlorobenzene-d4 9.72

Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 Butenol, methyl- 86 C5H10O 060766-00-9 42 2 3-hydroxy-4,4-dimethyl .gamma. B... 130 C6H10O3 052126-90-6 40 3 Cyclopropanemethanol, .alpha.-bu... 128 C8H160 004379-16-2 36 4 3-Buten-2-ol, 2-methyl- (CAS) $$... 86 C5H10O 000115-18-4 36 Abundance Scan 144 (5.018 min): 00321. D (-) m/z 43.10 100.00% 43 71

5000 59

| 53 MAAAAAA 4.60 4.80 5.00 5.20 5.40 85 0 ‘ +‘IF‘ ‘ I ' 1 . .Ijlll. ..,..1.1 4 ....................... 1. m/ z 71.10 98.39% /z-> 10 20 30 40 50 60 70 80 90 100 110 Abundance #4093: Butenol, methyl- 43 7h

5000 27 59 A 4.60 4.80 5.00 5.20 5.40 15 m/z 41.10 60.70% 53 ---------- —,l ■ • ■ i ■ •86 0 i ■ i ■ ■ ■ ■ i ■ r ■ ■ i ■ ■

m/z-> 10 20 30 40 50 60 701 80 90 100 110 Abundance #26149: 3-hydroxy-4,4-dimethyl .gamma. Butanolactone $$ Pa... 71 43 MALAA 4.60 4.80 5.00 5.20 5.40 5000 m/z 69.10 38.97% 57 31 ------------------------ 0 m/z-> 10 20 30 40 50 60 70I 80 90 100 110 Abundance #25047: Cyclopropanemethanol, aipha.-butyl- 7h A.. 11 . 1 4.60 4.80 5.00 5.20 5.40 43 m/z 59.10 34.96%

5000

27 57

0 1 ■ i ■ ' ' '"I 1 ' 11 I1' 1 1 1 I । + — 4 , 85 1 . ■ ■ i ■ . ' ■ I 1 ■ ■ ■ 110 i 1 1 ' ■ i 1 ' N , ,/) s, , ) 4 iz-> 10 20 30 40 50 60 701 80 90 100 110 4.60 4.80 5.00 5.20 5.40

00321.D SCAN508.M Mon Jan 14 10:46:42 2002 Page 5

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