GCMS results for sample AE00471, Jan 18 2002

NYC 9/11 Public Portal Document

Library Search Compound Report Data File : C:\MSDCHEM\1\5973N\02JAN10\00471.D Vial: 6 Acq On 10 Jan 2002 6:57 pm Operator: Sample : 508 scan ext 1/8 Inst : Instrumen Mise : January 10, 2002 Multiplr: 1.00 MS Integration Params: LSCINT.P Quant Method : C:\MSDCHEM\l-..\SCAN508.M (RTE Integrator) Title : 508 scan method Library : C:\DATABASE\WILEY7N.L Peak Number 3 Butenol, methyl- Concentration Rank 2 R.T. EstConc Area Relative to ISTD R.T. 5.01 0.50 ug/L 164603 1,4-Dichlorobenzene-d4 9.71

Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 Butenol, methyl- 86 C5H10O 060766-00-9 64 2 3-Buten-2-ol, 2-methyl- 86 C5H10O 000115-18-4 59 3 2(3H)-Furanone, dihydro-3-hydrox... 130 C6H10O3 052126-90-6 42 4 3-hydroxy-4,4-dimethyl .gamma. B... 130 C6H10O3 052126-90-6 42 Abundance Scan 143 (5.006 min): 00471 .D (-) m/z 71.10 100.00% 43 7h

5000 59 s AM o rr 53 1*i 1 1 1 1 1

n/z-> 0 1 ' i ' ' ■ ■ i ■ ' 1 ' i '

10 20 30 45 40 50 60 70 84 TPPPTTPTTP 80 90 100 110 120 130 4.60 m/ z 4.80 43.10 5.00 5.20 5.40 90.70% Abundance #4093: Butenol, methyl- 43 7h

AY- . Ax___ J . A >- \ A___ / 5000 59 ' I ' ' ' ' I ' ' ' ' I ' ' ' ' I ' ’ 1 ' I ' ' 27 4 60 4.80 5.00 5.20 5.40 15 m/z 41.10 73.97% 53 — I l 4 86 01 q-n1. 11" । । i । i i i i । ■ T’I 1 I 1 ’ 1 1 I ■ ‘ ■ i ■ ■ ■ ' i ' ' ' ' i ■ ■ ■ ' i ■ m/z-> 10 20 30 40 50 60 70 80 90 100 110 120 130 Abundance #4083: 3-Buten-2-ol, 2-methyl- 7h 43 - ■1 r1 i ' । 1' cerree । 4.60 4.80 5.00 5.20 5.40 5000 m/z 69.10 52.70% 59 27 53

m/z-> 0 0170001009137, 10 20 30 40 -l, 50 60 '' — 4 70) I ! , I | , 1^1 | 80 , ---FFFTPP , I 90 100 110 120 130 Abundance #26146: 2(3H)-Furanone, dihydro-3-hydroxy-4,4-dimethyl- 7 4.60 4.80 5.00 5.20 5.40 m/z 59.10 35.56% 43 5000

57

m/z-> 0 ....... .... ......... .. 1...................... 130 10 20 30 40 50 60 70) 80 90 100 110 120 130 - 4.60 4.80 .A. A 5.00 5.20 5.40

)0471.D SCAN508.M Fri Jan 11- 10:08:49 2002 Page 5

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