GCMS results for sample AE00464, Jan 24 2002

NYC 9/11 Public Portal Document Library Search compound Report

Data File : C:\MSDCHEM\1\5973N\02JAN11\00464.D Vial: 6 Acq Cn : 11 Jan 2002 6:15 pm Operator: Sample : 508 scan Inst : Instrumen Mise : January 11, 2002 Multiplr: 1.00 MS Integration Params: LSCINT.P Quant Method : C:\MSDCHEM\1... \SCAN508.M (RTE Integrator) Title : 508 scan method Library : C:\DATABASE\WILEY7N.L Peak Number 2 Butenol, methyl- Concentration Rank 2 R.T. EstConc Area Relative to ISTD R.T. 5.01 0.29 ug/L 92081 1,4-Dichlorobenzene-d4 9.72 Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 Butenol, methyl- 86 C5H10O 060766-00-9 56 2 3-Buten-2-ol, 2-methyl- 86 C5H10O 000115-18-4 56 3 Furan, tetrahydro-2-(methoxymeth. .. 116 C6H1202 019354-27-9 53 4 Butane, 2-bromo-2-methyl- $$ ter... 150 C5HllBr 000507-36-8 45 Abundance Scan 143 (5.006 min' : 00464.D (-) m/ z 71.10 100.00% 43 71

5000 59 AD m/z-> 0 ■

Abundance 10 I* 20 30 40 + 50 53

60 70 #4093: Butenol, methyl- 80 84...................................... 90 100 110 120 4.60 m/z 4.80 43.10 5.00 5.20 84.59% 5.40

43 7h Al \ A A / 5000 59 27 4.60 4.80 5.00 5.20 5.40 15 m/z 41.05 51.79% 53 0- ....... ....... 11 | _ — ’ I ' 1 ' ' I ' ' ' ' I ' ' ' ' I ' ' ' * I ' ' ' l ' 86 n/z-> 10 20 30 40 50 60 70 80 90 100 110 120 Abundance #4083: 3-Buten-2-ol, 2-methyl- 711 43 A/ , DW, 0. 4 60 4.80 5.00 5.20 5.40 5000 m/z 69.10 36.15% 27 59 N 53 -— miz-> 01 —10....201.. 111.37,1 30 40 50 60 70 80 90 86 ' i ' ■ 1 ' i ' ' ' ' i ' ■ ■ ' i ' ' ' ■ i ' 100 110 120 — Abundance #16750: Furan, tetrahydro-2-(methoxymethyl)- $$ 2-(Methoxy... ■ i ’ ■ 71 4.60 4.80 5.00 5.20 5.40 m/ z 59.10 34.98% 43 5000

27 58 n/z-> 0 1 • । ■ ■ ■ • । ■ * > • । ■ 10 20 30 4 40 1 1 1 **) । i1 1 50 60 70 1....................... .......... 116 80 90 100 110 120 . ............ ..................................... 4.60 4.80 5.00 5.20 5.40

00464.D SCAN508.M Mon Jan 14 10:47:01 2002 Page 4

NYC-WTC_000051446