GCMS results for sample AE00464, Jan 24 2002

NYC 9/11 Public Portal Document

Library Search Compound Report

Data File : C:\MSDCHEM\1\5973N\02JAN11\00464.D Vial: 6 Acq On : 11 Jan 2002 6:15 pm Operator: Sample : 508 scan Inst : Instrumen Mise : January 11, 2002 Multiplr: 1.00 MS Integration Params: LSCINT.P

Quant Method : C:\MSDCHEM\1...\SCAN508. M (RTE Integrator) Title : 508 scan method Library- : C:\DATABASE\WILEY7N.L ********************************************************************* Peak Number 1 2-Pentenal, (E)- Concentration Rank 6

R.T. EstConc Area Relative to ISTD R.T.

4.86 0.15 ug/L 47105 1,4-Dichlorobenzene-d4 9.72

Hit# Of 5 Tentative ID MW MolForm CAS# Qual

1 2-Pentenal, (E)- 84 C5H80 001576-87-0 25 2 2-Butenal, 2-methyl- (CAS) $$ 2-... 84 C5H80 001115-11-3 12 3 2H-Pyran, 3,4-dihydro- $$ .delta... 84 C5H80 000110-87-2 9 4 4-Pentenal (CAS) $$ 4-Pentenal- 84 C5H80 002100-17-6 9 Abundance Scan 130 (4.858 min): 00464.D (-) m/z 84.00 100.00%

N_ 84 55 5000 41 59

47 51 4.60 4.80 5.00 5.20 m/z-> 0 • i • ■ • ■ i • ■ • ■ i • • ■ • i ■ 20 25 30 35 40 19‘ H ■ • i ■ 45 50 55 60 65 70 75 80 85 90 । ■ ■ ■' । ■ m/z 55.10 68.23% Abundance #3201:2-Pentenal, (E)- 55 27 39 84 5000 4.60 4.80 5.00 5.20 m/ Z 83.10 50.75% 51 66 m/z-> 0 • ■ । ■ ■ ■ • । > 20 —35+ —..... Ill 25 30 35 40 45 50 55 60 65 70 75 80 85 ■ • i • • • > 11 • • • i ■ ■ ■ ■ i • • > > i • • 11 > *1 > । * > 90 Abundance #3214: 2-Butenal, 2-methyl- (CAS) $$ 2-FORMYL-2-BUTENE $$ ... 29 55

84 4.60 4.80 5.00 5.20 5000 39 m/z 41.10 50.66%

—26 50 0 ■ ।।. 1, —.... 4i T I | . . . . | I . | . I I | I . I I....... rn/z~> Abundance 20 25 30 35 40 45 50 55 60 65 70 75 80 85 #3369: 2H-Pyran, 3,4-dihydro- $$ .delta.(Sup2)-Dihydropyra... 90 _A 4.60 4.80 5.00 5.20 m/z 39.10 42.67% 27 84 5000

51 69 1 66 | 0 11111 > r>... ।1.. 11 >. ■ • ।....।. I'1'1111 ........... m/z-> 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 4.60 4.80 5.00 5.20

00464.D SCAN508.M Mon Jan 14 10:47:00 2002 Page 3

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