GCMS results for sample AE00464, Jan 24 2002

NYC 9/11 Public Portal Document

Llprary Searcn compound Report

Data File : C:\MSDCHEM\1\5973N\02JAN11\00464.D Vial: 6 Acq Cn : 11 Jan 2002 6:15 pm Operator: Sample : 508 scan Inst : Instrumen Mise : January 11, 2002 Multiplr: 1.00 MS Integration Params: LSCINT.P

Quant Method : C:\MSDCHEM\1... \SCAN508.M (RTE Integrator) Title : 508 scan method Library : C:\DATABASE\WILEY7N.L Peak Number 3 3-[.beta.-hydroxy-(.beta.,.. Concentration Rank 4

R.T. EstConc Area Relative to ISTD R.T. 5.71 0.19 ug/L 60621 1,4-Dichlorobenzene-d4 9.72

Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 3-[.beta.-hydroxy-(.beta.,.beta.... 86 C5H6D2O 005557-87-9 43 2 2-Butene, 1-methoxy-, (E)- 86 C5H10O 010034-14-7 42 3 Pentane, 2-methyl- $$ Isohexane ... 86 C6H14 000107-83-5 38 4 2-Furanmethanol, tetrahydro- (CA... 102 C5H10O2 000097-99-4 37 Abundance Scan 205 (5.714 min): 00464.D (-) m/z 43.10 100.00% 43 71

5000 39

84 540 5.60 5.80 6.00 i ‘■ r " 111" ' i ■1' ■ i' Or - m/z 41.10 95.88% n/z-> 5 10 15 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 Abundance #3392: 3-[ beta.-hydroxy-(.beta.,.beta.-dideuterio)]ethylp...

5000 71 _ A ,I 58 85 5.40 5.60 5.80 6.00 68 53 m/z 71.00 92.15% 44 —

... AM Or < ‘ < i * ■ ■ ■। • ■ •• । •■ ■ ■ । ■ ■ ■ ■ । ■ • ■ ■ । > ■ • ■ । i" I ।........... HI....... TTT rn/z-> 5 10 15 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 Abundance #4112:2-Butene, 1 -methoxy-, (E)- 71 41 5.40 5.60 5.80 6.00 5000 27 55 m/z 69.10 54.30% 45 86

■n/z-> Oh 5 i'" ' r " ' i " '' I 33 i" " i" 10 15 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 m +9- Iapevnee ■111' > ■ ■ ।1 • * 11 ■

Abundance #4253: Pentane, 2-methyl- $$ Isohexane $$ 2-Methylpentane... 43 5.40 5,60 5.80 6.00 m/z 39.10 46.37%

5000 27 71 39 15 57

n/z-> — 0b .. I....... 86 ThT " r " ' i" 5 10 15 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 +53L r "' i V —————— 5.40 5.60 5.80 6.00

00464.D SCAN508.M Mon Jan 14 10:47:01 2002 Page 5

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