GCMS blank analysis results for sample AE00327, Jan 2002

NYC 9/11 Public Portal Document

Llprary Searcn compound Report

Data File : C:\MSDCHEM\1\5973N\02JAN10\0108B.D Vial: 1 Acq On : 10 Jan 2002 12:21 pm Operator: Sample : lab blank ext 1/8 Inst : Instrumen Mise : January 10, 2002 Multiplr: 1.00 MS Integration Params: LSCINT.P Quant Method : C:\MSDCHEM\1...\SCAN508.M (RTE Integrator) Title : 508 scan method Library : C:\DATABASE\WILEY7N.L

Peak Number 2 3-Buten-2-ol, 2-methyl- Concentration Rank 7 R.T. EstConc Area Relative to ISTD R.T. 5.01 0.11 ug/L 34993 1,4-Dichlorobenzene-d4 9.71

Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 3-Buten-2-ol, 2-methyl- 86 C5H10O 000115-18-4 80 2 Butenol, methyl- 86 C5H10O 060766-00-9 42 3 3-Buten-2-ol, 2-methyl- 86 C5H10O 000115-18-4 39 4 2-Furanmethanol, tetrahydro- (CA... 102 C5H10O2 000097-99-4 38 Abundance Scan 143 (5.006 min): 0108B.D (-) m/z 43.10 100.00% 4B 71

5000

39 55 59 NW A N 4.60

n/z-> Of 5 ■ ■ i - ■

10 m.. Il. 15 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 ■ ■ i ■ • 84 mlpy....... m/ z 4.80 71.10 5.00 5.20 90.10% 5.40

Abundance #4085: 3-Buten-2-ol, 2-methyl- 71 43

5000 59 AXA 4.60 4.80 5.00 5.20 5.40 27 31 m/ z 41.10 71.94% 53 0 ‘ I "11" " I" ■ ■ i " " i1 ■ " i' " ' i1 H 671 ■11 < 1111 ! ■ > । < • ■ ■।।1। 86 ।

_N m/z-> 5 10 15 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 Abundance #4093: Butenol, methyl- 43 71

4 60 4.80 5.00i 5.20 5.40 5000 59 m/Z 69.10 59.33% 27 15 31 53 671 ,................. 86............ 01 " ।" i ’ TTI ■ < i'1" i" • I''11111 111' । T ophaly 1" I " " I " 111" " 11" 11 nz-> 5 10 15 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 Abundance #4084: 3-Buten-2-ol, 2-methyl- 71 460 4.80 5.00 5.20 5.40 43 m/z 59.10 32.70%

5000 59

27 67 86 Of -mm ■ > > ■ । ■ 1111 1..................11.............. ■ t ■ • • ■ i • ■ ‘ ‘ i •' • • r1 m/z-> 5 10 15 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 4.60 4.80 5.00 5.20 5.40

108B.D SCAN508.M Fri Jan 11 10:09:14 2002 Page 4

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