GCMS surrogate recovery results for sample AE03184, March 2002

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Analytical report showing surrogate recovery data for sample AE03184 analyzed on March 15, 2002.

NYC-WTC_000006045–000006064

Folder label: “GCMS X 2/12/02 A 3/01/02”

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NYC 9/11 Public Portal Document Llprary searcn Compound Report

Data File : C:\MSDCHEM\l\5973N\02MAR01\03184.D Vial: 4 Acq Oh : 1 Mar 2002 12:48 pm Operator: Sample : 508 scan Inst : Instrumen Mise : March 1, 2002 Multiplr: 1.00 MS Integration Params: LSCINT.P Quant Method : C:\MSDCHEM\1...\HP022102.M (RTE Integrator) Title : 508 scan method Library : C:\DATABASE\WILEY7N.L ********************************************************************* Peak Number 7 Butenol, methyl- Concentration Rank 9

R.T. EstConc Area Relative to ISTD R.T. 5.02 0.06 ug/L 21857 1,4-Dichlorobenzene-d4 9.71 Hit# Of 5 Tentative ID MW MolForm CAS# Qual

1 Butenol, methyl- 86 C5H10O 060766-00-9 50 2 3-Buten-2-ol, 2-methyl- (CAS) $$... 86 C5H10O 000115-18-4 9 , 3 2-Bromo-l-hexenoxide 178 C6HllBrO 000000-00-0 9 4 Di-iso-amyl oxalate 230 C12H2204 000000-00-0 9 Abundance Scan 146 (5.022 min): 03184.D (-) m/Z 43.10 100.00% 43 71

5000 59 207 4.60 4.80 5.00 5.20 5.40 86 0- I' ‘1'r ■" i""I"11,T1" 111" T h 111111 m/z 71.00 78.18% i" " i" " r' " i " " i" " i" " i" " r ‘ " r " ‘ r ■ " r •1111'1 niz-> 10 2030405060 70 8090 100 110 120 130 140 150 160 170 180 190 200210 Abundance #4093: Butenol, methyl- 43 71

5000 59 27 4.60 4.80 5.00 5.20 5.40 15 m/z 41.10 54.26%

...... ..... „.ll|| ! , 86 0- .... "i"" i" "i "“i"" i'"'I 1" 11"1 ■ i''" i" " i " " i" " i'"' r1" i" " i " " i1" ■ i" " i" " r "1 r " m/z-> 10 20 30 40 50 60 70 80 90 100110120130140150160170180190200210 Abundance #4090: 3-Buten-2-ol, 2-methyl- (CAS) $$ 2-Methyl-3-buten-2... 43 71 ........AAA// ■ ■ i 1 ’ TI 1111 1 11 1 1 r1 1 4.60 4.80 5.00 5.20 5.40 5000 m/ Z 59.10 35.74% 27 59

, 86 0 | J''I UI 1*1 IUI| i > ■ ■ i ■ ■' ■ i ■ ■ ■ ■ i ■ ■ ■' i ‘' i ■ ‘■ i1"' i ■"' i' ■'' i" " I'1 ■ ■ i" " I ■' " i'"' i ‘" mfe-> 10 20 30 40 50 60 70 80 90 100110120130140150160170180190200210 Abundance 41 71 #82608:2-Bromo-1-hexenoxide i ■ 1 1 ■ i ■ 4.60 4.80 5.00 Aoini"— 5.20 5.40 m/z 69.10 35.42% 55 5000 81

107 , ...... I II - 0 .............. I 149 177 ''i""r■"r"'i'’ ’I’ 1"i'■ ’ I’ ।>11'।>11>।■ ।[11.,।. 11!1210010011111111"51701501000100000101110013 i ■ ■ ' ■ i ' n/z-> 10 20 30 40 50 60 70 80 90 100110120130140150160170180190200210 4.60 4.80 5.00 5.20 5.40

)3184.D HP022102.M Mon Mar 04 12:32:53 2002 Page 9

NYC-WTC_000006057

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Laboratory report documenting gas chromatography-mass spectrometry analysis of environmental sample AE03247 conducted on March 15, 2002.

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