GCMS surrogate recovery results for sample AE03184, March 2002

NYC 9/11 Public Portal Document Library Search Compound Report

Data File : C:\MSDCHEM\l\5973N\02MAR01\03184.D Vial: 4 Acq On : 1 Mar 2002 12:48 pm Operator: Sample : 508 scan Inst : Instrumen Mise : March 1, 2002 Multiplr: 1.00 MS Integration Params: LSCINT.P Quant Method : C:\MSDCHEM\1...\HP022102.M (RTE Integrator) Title : 508 scan method Library : C:\DATABASE\WILEY7N.L ********************************************************************* Peak Number 8 Hexanal (CAS) $$ n-Hexanal ... Concentration Rank 11 R.T. EstConc Area Relative to ISTD R.T. 5.11 0.06 ug/L 20556 1,4-Dichlorobenzene-d4 9.71 Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 Hexanal (CAS) $$ n-Hexanal $$ He... 100 C6H120 000066-25-1 38 2 Hexanal 100 C6H120 000066-25-1 38 3 Acetic acid, chloro-, butyl este... 150 C6H11C1O2 000590-02-3 10 4 Butanal, 2-methyl- (CAS) $$ 2-Me... 86 C5H10O 000096-17-3 9 Abundance Scan 154 (5.112 min): 03184.D (-) m/z 44.0.0 100.00% 44 56

5000

51 86 4.80 5.00 5.20 5.40 0 i"" i" " r ‘ "i" " I" " r'" i I’ TTttt " I' ‘'11 " " r " 11 " " I 1 " 1 I' " 11"1 I > I 11 11 i u I 1111 m/z 56.10 69.37% rn/z—> 5 10 15 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 100105 Abundance #8200: Hexanal (CAS) $$ n-Hexanal $$ Hexaldehyde $$ Caproa... 44 56

5000 4.80 5.00 5.20 5.40 39 72 m/z 41.10 68.95% 82 | 100 0 " ■■ i'1' 'i p-rTTp+njTTTTp-rrTJ^^ /z—> 5 10 15 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 100105 Abundance #8186: Hexanal 44 56 4.80 5.00 5.20 5.40 AAAAAA 5000 m/a 57.00 58.14% 27

67 72 82

/z-> 0 "I"... TIIapamu 5 10 15 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 100105 mm 100 Abundance #45733: Acetic acid, chloro-, butyl ester (CAS) $$ n-Butyl... ■ 1 1 i ■ ■ ■ ■ i ■ ' ' r i ■ ■ ■ ■ i ■ 1 1 1 i 29 55 4.80 5.00 5.20 5.40 41 m/z 43.10 46.37%

5000 70 49 15 79

m/z—> 0 - TTP - l""l' 5 10 15 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 100105 — mm 4.80 5.00 5.20 5.40

>3184.D HP022102.M Mon Mar 04 12:32:53 2002 Page 10

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