GCMS analysis results for sample AE00614, Feb 2002

NYC 9/11 Public Portal Document

Library Search Compound Report

, Data File : C:\MSDCHEM\1\5973N\02JAN29\00614.D Vial: 3 Acq On : 29 Jan 2002 4:17 pm Operator: Sample : 508 scan Inst : Instrumen Mise : January 29, 2002 Multiplr: 1.00 MS Integration Params: LSCINT.P Quant Method : C:\MSDCHEM\1...\SCAN508.M (RTE Integrator) Title : 508 scan method Library : C:\DATABASE\WILEY7N.L ********************************************************************* Peak Number 2 1-CHLOROHEXA-5-YNE $$ 1-Hex... Concentration Rank 7

R.T. EstConc Area Relative to ISTD R.T.

4.63 0.14 ug/L 69995 1,4-Dichlorobenzene-d4 9.72

Hit# Of 5 Tentative ID MW MolForm CAS# Qual

1 1-CHLOROHEXA-5-YNE $$ 1-Hexyne, . 116 C6H9C1 010297-06-0 38 2 Butanoic acid, 2-methyl-, methyl... 116 C6H1202 000868-57-5 35 3 Butanoic acid, 2-methyl-, methyl... 116 C6H1202 000868-57-5 25 4 Butanoic acid, 2-methyl-, methyl... 116 C6H12O2 000868-57-5 25 Abundance Scan 110 (4.629 min): 00614. D (-) m/z 71.00 100.00% 71 41 88 57 5000 101 A A ... II‘‘‘IY — ■ > i ■ ■ . T 4.20 m/z 4.40 41.10 4.60 4.80 5.00 78.80% m/z-> 20 30 40 50 60 70 80 90 100 110 120 Abundance #16344:1-CHLOROHEXA-5-YNE $$ 1-Hexyne, 6-chloro- (CAS) $$...

WAAL 88 39 81

5000 54 4.20 4.40 4.60 4.80 5.00 67 m/z 88.00 75.30%

■ । • • ■ ■ । ■ 49 i 1 1 1 ....1 .... 1 ■ ■ i ’ ■ ■ ■ । ■ ■ • ■ । ■ ■ 101........ n/z-> 20 30 40 50 60 70 80 90 100 110 120 Abundance #16435: Butanoic acid, 2-methyl-, methyl ester 57 83 AAMAA .A 4.20 4.40 4.60 4.80 5.00 5000 m/ z 57.10 61.79% 101 27 69 | 33 i___________ +1 । , । ■ ■ ■ • । 116 ‘I’’ 1 1 1 1 ' UGTUTTT "ll > i ■ > > • । ■ ■ i ■ >■ i ■ ■ m/z-> 20 30 40 50 60 70 80 90 100 110 120 Abundance #16438: Butanoic acid, 2-methyl-, methyl ester r1 ' ■ ' i ■ ■ 57 4.20 4.40 4.60 4.80 5.00 88 41 m/z 43.10 47.58%

5000

n/z—> 20 30 40 I1 T 50 .. ...........

60 70 80 90 101

100 110 120 NAkdl 4.20 4.40 4.60 4.80 5.00

30614 .D SCAN508.M Wed Jan 30 09:02:15 2002 Page 4

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