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GCMS analysis results for sample AE00614, Feb 2002

Machine-extracted title · confidence 100%

Laboratory report showing GCMS analysis results for sample AE00614 conducted on February 1, 2002.

NYC-WTC_000051605–000051623

Folder label: “GCMS X 1/9/02 A 1/29/02

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NYC 9/11 Public Portal Document

Library Search Compound Report . Data File : C:\MSDCHEM\1\5973N\02JAN29\00614.D Vial: 3 Acq On : 29 Jan 2002 4:17 pm Operator: Sample : 508 scan Inst : Instrumen Mise : January 29, 2002 Multiplr: 1.00 MS Integration Params: LSCINT.P Quant Method : C:\MSDCHEM\l-..\SCAN508.M (RTE Integrator) Title : 508 scan method Library : C:\DATABASE\WILEY7N.L * ************************************************************** ** ★ * * * Peak Number 1 2,2-Dimethoxybutane Concentration Rank 4 R.T. EstConc Area Relative to ISTD R.T. 4.24 0.20 ug/L 99352 1,4-Dichlorobenzene-d4 9.72 Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 2,2-Dimethoxybutane 118 C6H14O2 003453-99-4 35 2 2-Butenoic acid, (Z)- (CAS) $$ 1... 86 C4H602 000503-64-0 27 3 2-Propenoic acid, 2-methyl- (CAS... 86 C4H6O2 000079-41-4 27 4 N,N'-Diacetylethylenediamine 144 C6H12N202 000871-78-3 23 Abundance Scan 76 (4.241 min): 00614.D (-) m/z 85.00 100.00% 43 85

5000 55 60 A 1 ' I • ’

37 71 103 3.80 4.00 4.20 4.40 4.60

m/z-> -mmP -H 49 I""! "..... . mmmP I

20 25 30 35 40 45 50 55 60 65 70 75 80 85 30 95 100 105110 ' 1' m/ z 43.10 84.43% Abundance #17888: 2,2-Dimethoxybutane 87 55

5000 40 45 A 3.80 4.00 4.20 4.40 Mw 4.60 27 m/z 41.10 77.55%

A 103 33 92 i ’" ■ i TH > • l •' • > l ■ > > • 11111111 > > I •11111 HT ' i"1 ■ i11H i11 n/z-> 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 100 105 110 Abundance #3731: 2-Butenoic acid, (Z)- (CAS) $$ Isocrotonic acid $$ ... 85

39 3.80 4.00 4.20 4.40 4.60 5000 m/z 87.10 66.37% 68 27 . 45

m/z-> „20.251.. 57 ■ i" " i ■1" i" ‘ ■ i" 30 35 40 45 50 55 60 65 70 75 80 85 90 95 100 105 110 I ■" r " 11'1'' i" " r " ■ i

Abundance #3758: 2-Propenoic acid, 2-methyl- (CAS) $$ Methacrylic ac... | i y | i I r I Ji > I । | i , . । । । । 41 85 3.80 4.00 4.20 4.40 4.60 m/z 89.10 56.28%

5000

69

n/z—> 1 ’ 1 •" 111' " I'" 11'1' + .. I"1'! 58 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 100 105 110 ...... ..... . —mmmmmpmp 3.80 4.00 4.20 4.40 4.60

30614 .D SCAN508.M Wed Jan 30 09:02:14 2002 Page 3

NYC-WTC_00005161 1

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NYC-WTC_000051611Source: NYC Law Department, mirrored locally

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DEP GCMS data table, Jan-Feb 2002 · Box DEP Box 12

NYC-WTC_000003981

Multi-page laboratory data sheet containing sample analysis results and metadata for DEP GCMS records from January to February 2002.

1 shared non-person entities · 1 shared topics · similarity 0.997

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