GCMS blank results for sample AE03611, March 28, 2002

NYC 9/11 Public Portal Document

Library Search Compound Report * Data File : C:\MSDCHEM\1\5973N\02MAR08\03611.D Vial: 1 Acq On : 8 Mar 2002 3:35 pm Operator: Sample : 508 scan Inst : Instrumen Mise : March 8, 2002 Multiplr: 1.00 MS Integration Params: LSCINT.P Quant Method : C:\MSDCHEM\l..-\HP022102.M (RTE Integrator) Title : 508 scan method Library : C:\DATABASE\WILEY7N.L ********************************************************************* Peak Number 3 2,2-dimethoxybutane Concentration Rank 4

R.T. EstConc Area Relative to ISTD R.T.

4.24 0.13 ug/L 63323 1,4-Dichlorobenzene-d4 9.71

Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 2,2-dimethoxybutane 118 C6H14O2 003453-99-4 83 2 2,2-Dimethoxybutane 118 C6H14O2 003453-99-4 78 3 N-Methyl-2-hydroxyheptanoic acid... 159 C8H17N02 087919-97-9 42 4 1,3-Dioxane (CAS) $$ m-Dioxane $..♦ 88 C4H802 000505-22-6 9 Abundance Scan 77 (4.243 min): 03511 .D (-) m/ z 87.10 100.00% 87 55 43 5000 i ■ ■ • ‘ i • ■ ■ > i 1 ■ • ■ i • * *'' i ! r“'_ . 71 103 3.80 4.00 4.20 4.40 4.60 miz-> 0 ....... I— ,l.... ... I 11 1 ‘ I 20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 i ‘ ‘ ‘ ‘ ! T m/z 89.00 77.38% Abundance #17889:2,2-dimethoxybutane 55 87

5000 45 3.80 4.00 4.20 4.40 4.60 27 m/z 55.00 71.46% 103

miz-> —l 01 »I.»»11.1»»11 l.lI I I ‘‘*1I »•»«(« 20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 T I*•’* I

Abundance #17888:2,2-Dimethoxybutane 87 55 . A • • i * • 3.80 4.00 4.20 4.40 4.60 m/z 43.00 58.45%

N 5000 45 27 103 O-1T • • i 34 _ •1'1 ‘1,11 ■' ■ ■ i ■ " ‘ i ■ — 44 ----- mlz-> 20 30 40 50 60 70 80 90 00 110 120 130 140 150 160 Abundance #58743: N-Methyi-2-hydroxyheptanoic acid amide $$ Heptanam... 55 89 3.804.00 4.20 4.40 4.60 AADA m/z 45.00 A 14.47%

5000 41

101 159 O-TI , I m/z—> 20 30 40 50 60 70.80 90 100 do 120 130 140 150 160 3.80 4.00 4.20 4.40 4.60

03511.D HP022102.M Fri Mar 15 10:09:10 2002 Page 5

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