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GCMS DFTPP calibration report, Feb 5 2002

Machine-extracted title · confidence 95%

Chromatogram and method report for DFTPP calibration verification conducted on February 5, 2002.

NYC-WTC_000004770–000004933

Folder label: “GCMS X 2/1/02 A 2/5/02

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Scanned page image, NYC-WTC_000004922
OCR text

OCR status: ok · source: pdftotext

NYC 9/11 Public Portal Document Library Search Compound Report Data File : C:\MSDCHEM\1\5973N\02FEB05\30648A.D Vial: 5 ' Acq On 5 Feb 2002 2:03 pm Operator: Sample : 508 scan; re-ext Inst : Instrumen Mise : February 5, 2002 Multiplr: 1.00 MS Integration Params: LSCINT.P

Quant Method : C:\MSDCHEM\1...\HP020702.M (RTE Integrator) Title : 508 scan method Library : C:\DATABASE\WILEY7N.L ********************************************************************* Peak Number 3 2,2-dimethoxybutane Concentration Rank 1 R.T. EstConc Area Relative to ISTD R.T. 4.24 0.54 ug/L 412344 1,4-Dichlorobenzene-d4 9.71 Hit# Of 5 Tentative ID MW MolForm CAS# Qual 1 2,2-dimethoxybutane 118 C6H14O2 003453-99-4 64 2 2,2-Dimethoxybutane 118 C6H14O2 003453-99-4 43 3 Methyl l-Methyl-d3-2-propenyl Ether 89 C5H7D3O 000000-00-0 36 4 Glycine, methyl ester $$ NH2CH2C... 89 C3H7NO2 000616-34-2 9 Abundance Scan 76 (4.241 min): 30648A.D (-) m/z 87.10 100.00% 87

55 5000 43

103 3.80 4.00 4.20 4.40 4.60 711 - O+ pp + 1111 j 1111 111" ■ ... I....... m/z 89.10 87.26% miz-> 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 100 105 110 Abundance #17889:2,2-dimethoxybutane 55 87

5000 27 45 3.80 4.00 4.20 4.40 4.60 "/Z 55.10 54.13% 92 103 33 11" I' " 1 mhmmmmmmm H " ।1 ■1' ।"1 • ।" 01 " i" ■' i ■ TTTHTTTTTT m/z-> 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 100 105110 Abundance #17888:2,2-Dimethoxybutane 87 55 AAm . A... 3.80 4.00 4.20 4.40 4.60 5000 m/z 43.10 46.84% 45 27 40

92 103 33 0! " i “ " i' "I'.. . i" " r '" i' ■" i'1" i HP ■ । ■ ■H । ■ ■' ■ । m/z-> 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 100 105110 Abundance #4232: Methyl 1-Methyl-d3-2-propenyl Ether i ■ ■f ■ i ■ ° ■ । ■ 151 101110/01 89 3.80 4.00 4.20 4.40 4.60 m/z 45.10 15.57% 71 5000

m/z-> 46 ,59., 0 1111111100011—0011—029000—00——um ।1111111111111111 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 100 105110 "TT | I I I I | 1 I I I | I I 1 1 | I ! > -- —A 3.80 4.00 4.20 4.40 4.60

30648A.D SCAN508.M Thu Feb 21 10:19:04 2002 Page 5

NYC-WTC_000004922

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NYC-WTC_000004922Source: NYC Law Department, mirrored locally

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