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GCMS analysis results for sample AE00614, Feb 2002

Machine-extracted title · confidence 100%

Laboratory report showing GCMS analysis results for sample AE00614 conducted on February 1, 2002.

NYC-WTC_000051605–000051623

Folder label: “GCMS X 1/9/02 A 1/29/02

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NYC 9/11 Public Portal Document

Library Search Compound Report . Data File : C:\MSDCHEM\1\5973N\02JAN29\00614.D Vial: 3 Acq On : 29 Jan 2002 4:17 pm Operator: Sample : 508 scan Inst : Instrumen Mise : January 29, 2002 Multiplr: 1.00 MS Integration Params: LSCINT.P Quant Method : C:\MSDCHEM\1...\SCAN508 . M (RTE Integrator) Title : 508 scan method Library : C:\DATABASE\WILEY7N.L ***************************************************************** * * * * Peak Number 3 2-Butenal, 3-methyl- $$ Cro... Concentration Rank 3 R.T. EstConc Area Relative to ISTD R.T.

4.83 0.21 ug/L 104221 1,4-Dichlorobenzene-d4 9.72

Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 2-Butenal, 3-methyl- $$ Crotonal... 84 C5H8O 000107-86-8 52 2 2-Butenal, 3-methyl- (CAS) $$ 3-... 84 C5H80 000107-86-8 52 3 Furan, 2,3-dihydro-4-methyl- (CA... 84 C5H8O 034314-83-5 50 4 2-Ethylacrolein $$ 2-Ethacrolein... 84 C5H8O 000922-63-4 47 Abundance Scan 128 (4.835 min): 00614.D (-) m/z 84.00 100.00% 84 55 59

41 5000

4.40 4.60 4.80 5.00 5.20 TH ,4 4791, l " > > l ........... TIT 38 i 71 88 '' I''' ' I' ■ 1' I'' '' I' ■ । 11 > • ■ ■ । • • ■ ■ । > m/z 59.10 83.16% /z-> 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 Abundance #3222: 2-Butenal, 3-methyl- $$ Crotonaldehyde, 3-methyl- $... 84 55

5000 39 .....4.601 ...4.80|.. — A— 27 4.40 5.00 5.20 m/z 55.10 80.00% 44 51 | 69 " I " '1111 .......... I1'1' । " 11" 1111 11' 1111111111111 ’ | ■ । । । | ‘ ' । I | ! /z-> 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 Abundance #3221: 2-Butenal, 3-methyl- (CAS) $$ 3-Methyl-2-butenal 84 55 A,., MW 4.40 4.60 4.80 5.00 5.20 5000 39 m/ z 41.10 62.19% 27

ANa 51 r' i1 ■ ' ■ i 1 44 " I " " I " 1 I " 1 ' I iT — 1 11111"" I rrrl69 m TFPTT _85111119011 1'95111' n/z-> 20 25 30 35 40 45 50 55 60 65 70 75 80 Abundance #3351: Furan, 2,3-dihydro-4-methyl- (CAS) $$ 4-METHYL-2,3-... 55 84 4.40 4.60 4.80 5.00 5.20 m/z 39.10 51.39%

5000 41

69

/z-> ' r ■ ■ 1 r ' 1 111' ‘111 20 25 30 35 44 - 40 51 45 50 4 m 55 60 65 70 75 80 85 90 95 111' ■ r ■'111 4.40 4.60 4.80 5.00 5.20

10614.D SCAN508.M Wed Jan 30 09:02:15 2002 Page 5

NYC-WTC_000051613

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NYC-WTC_000051613Source: NYC Law Department, mirrored locally

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DEP GCMS data table, Jan-Feb 2002 · Box DEP Box 12

NYC-WTC_000003981

Multi-page laboratory data sheet containing sample analysis results and metadata for DEP GCMS records from January to February 2002.

1 shared non-person entities · 1 shared topics · similarity 0.997

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