GCMS analysis results for sample AE00614, Feb 2002

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Laboratory report showing GCMS analysis results for sample AE00614 conducted on February 1, 2002.

NYC-WTC_000051605–000051623

Folder label: “GCMS X 1/9/02 A 1/29/02”

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NYC 9/11 Public Portal Document

Library Search Compound Report . Data File : C:\MSDCHEM\1\5973N\02JAN29\00614.D Vial: 3 Acq On : 29 Jan 2002 4:17 pm Operator: Sample : 508 scan Inst : Instrumen Mise : January 29, 2002 Multiplr: 1.00 MS Integration Params: LSCINT.P Quant Method : C:\MSDCHEM\1...\SCAN508.M (RTE Integrator) Title : 508 scan method Library : C:\DATABASE\WILEY7N. L ********************************************************************* Peak Number 4 3-Buten-2-ol, 2-methyl- (CA... Concentration Rank 5 R.T. EstConc Area Relative to ISTD R.T. 5.02 0.17 ug/L 84825 1,4-Dichlorobenzene-d4 9.72 Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 3-Buten-2-ol, 2-methyl- (CAS) $$... 86 C5H10O 000115-18-4 78 2 3-Buten-2-ol, 2-methyl- 86 C5H10O 000115-18-4 72 3 3-hydroxy-4,4-dimethyl .gamma. B... 130 C6H10O3 052126-90-6 64 4 2-Furanmethanol, tetrahydro- (CA... 102 C5H10Q2 000097-99-4 59 Abundance Scan 144 (5.018 min): 00614.D (-) m/ z 43.10 100.00% 43 71

5000 59 39 55 MA 5 14,4 „A , 4.60 4.80 5.00 5.20 5.40

nlz-? 20 '111 TTrrr‘1111191 + "TT - 51 I 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 1 l.... 11 । 67 I '1 ' i 1 ■' ■ i ■ ' ■1 i ' ■ '1 i '' 1' i 84 m/z 71.10 95.92% Abundance #4088: 3-Buten-2-ol, 2-methyl- (CAS) $$ 2-Methyl-3-buten-2... 7h

5000 An ,6., .. ........ 59 4.60 4.80 5.00 5.20 5.40 m/z 41.10 54.93% 53 0............... • > • > । • r • < 111111111 ——67 , 85 T ......... . 1 ■ ■ i' ■ ■ ■ i ■' ■11 ■ ■1 ■ I ■'111 m/z-> 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95

ANL Abundance #4084: 3-Buten-2-ol, 2-methyl- 71 43 - 4.60 4.80 5.00 5.20 5.40 5000 m/z 69.10 36.45% 59

27 67 86 ■ ■ i' ' ।'' ■' । ■ ■ ■' । ■' ■ ■ । •1 TTT ............... I —1ITTTTT ■ ■ ■ 11 ■ ■ ■ । ■ i /z-> 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 Abundance #26149: 3-hydroxy-4,4-dimethyl .gamma. Butanolactone $$ Pa...

43 71 4.60 4.80 5.00 5.20 5 40 m/ z 59.10 33.89%

5000

57 31 53 68 ■ ■ ।' ■ ■ ■ । ■111111111111111 11 " 1' i1' ।111 111' ■ 111 ■' I ■ i ■ 1IPPP —4.60A / A — m/z-> 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 4.80 5.00 5.20 5.40

)0614.D SCAN508.M Wed Jan 30 09:02:15 2002 Page 6

NYC-WTC_000051614

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Laboratory report showing GCMS analysis results for sample AE00616 conducted on February 1, 2002.

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