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← Document results/DEP Box 28/GCMS X 1/9/02 A 1/29/02
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GCMS analysis results for sample AE00614, Feb 2002

Machine-extracted title · confidence 100%

Laboratory report showing GCMS analysis results for sample AE00614 conducted on February 1, 2002.

NYC-WTC_000051605–000051623

Folder label: “GCMS X 1/9/02 A 1/29/02”

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Scanned page image, NYC-WTC_000051615
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OCR status: ok · source: pdftotext

NYC 9/11 Public Portal Document

Library Search Compound Report Data File : C:\MSDCHEM\1\5973N\02JAN29\00614.D Vial: 3 Acq On : 29 Jan 2002 4:17 pm Operator: Sample : 508 scan Inst : Instrumen Mise : January 29, 2002 Multiplr: 1.00 MS Integration Params: LSCINT.P Quant Method : C:\MSDCHEM\1...\SCAN508.M (RTE Integrator) Title : 508 scan method Library : C:\DATABASE\WILEY7N.L ********************************************************************* Peak Number 5 Acetic acid, 3-[1,3]dioxola... Concentration Rank 1 R.T. EstConc Area Relative to ISTD R.T. 5.89 3.89 ug/L 1922470 1,4-Dichlorobenzene-d4 9.72

Hit# of 5 Tentative ID MW MolForm . CAS# Qual

1 Acetic acid, 3-[1,3]dioxolan-2-y... 174 C8H14O4 000000-00-0 33 23-(CYCLOHEX-3'-EN-YL)PROPANOL $$... 174 C8H14O4 015745-87-6 33 3 Silane, tetramethyl- 88 C4H12Si 000075-76-3 25 4 Silane, tetramethyl- (CAS) $$ Te... 88 C4H12Si 000075-76-3 9 Abundance Scan 220 (5.885 min): 00614.D (-) m/z 73.10 100.00% 7)3

5000 43 5.60 5.80 6.00 6.20 I' • ’' I ‘‘ I —l TTTTTTTTf 55 t 11 87 103 ' I '' ■ I'''1 j'''' I 11''11 m/z 43.10 24.68% m/z-> 10 20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 Abundance #78238: Acetic acid, 3-[1,3]dioxolan-2-ylpropyl ester 70

5000 —nB—mmTuuut 5.60 5.80 6.00 6.20 43 m/z 45.10 9.54% 27 55 87 113 174 T-rp- ■ i1।1 TTTT *100‘u"uuun—nU*3g '11'11 ■ i ■'' ■ i' mlz-> 10 20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 Abundance #36138: 3-(CYCLOHEX-3'-EN-YL)PROPANOL $$ 2-Cyclohexene-1-p... 73 5.60 5.80 6.00 6.20 5000 m/z 41.10 9.38%

27 55 43 87 113 TTTTTTTTT ■ r ■ ■ ‘ i " '' i1 r " 1' I " ‘' I" ‘' 11" (1111111 ’1 ‘ 111 ITT 174 I' " 11 An y .n .■ miz-> 10 20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 Abundance #4814: Silane, tetramethyl- —BdTmr 70 5.60 5.80 6.00 6.20 m/ z 71.10 6.90%

5000

45 | 53 15 88 111'11 " 1 r THPTTT " i " 1' i11111" " i ■ " 11 1' " 11 V ■ ■ i ■ A 1

m/z~> 10 20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 5.60 5.80 6.00 6.20

)0614.D SCAN508.M Wed Jan 30 09:02:15 2002 Page 7

NYC-WTC_000051615

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NYC-WTC_000051615Source: NYC Law Department, mirrored locally

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