GCMS results for sample AE00467, Jan 24 2002

NYC 9/11 Public Portal Document

Library Search Compound Report Data File : C:\MSDCHEM\1\5973N\02JAN11\00467.D Vial: 7 Acq On : 11 Jan 2002 7:05 pm Operator: Sample : 508 scan Inst : Instrumen Mise : January 11, 2002 Multiplr: 1.00 MS Integration Params: LSCINT.P Quant Method : C:\MSDCHEM\1...\SCAN508.M (RTE Integrator) Title : 508 scan method Library : C:\DATABASE\WILEY7N. L ********************************************************************* Peak Number 1 Acetic acid, 3-[1,3]dioxola... Concentration Rank 2

R.T. EstConc Area Relative to ISTD R.T. 5.89 4.18 ug/L 1509230 1,4-Dichlorobenzene-d4 9.72 Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 Acetic acid, 3-[1,3]dioxolan-2-y... 174 C8H14O4 000000-00-0 33 2 3-(CYCLOHEX-3 ‘ -EN-YL)PROPANOL $$.. . 174 C8H14O4 015745-87-6 33 3 Silane, tetramethyl- 88 C4H12Si 000075-76-3 25 4 N-Ethylformamide $$ N-Formylethy... 73 C3H7NO 000627-45-2 9 Abundance Scan 220 (5.886 min): 00467.D (-) m/ z 73.10 100.00% 73

m/z-> 5000

0 • i • ■ ■ ■ i ......... ...... 43

■ • ■11 • ■ • >.................. i ′′′ ■ । ■ ■ 87 103 । ■ ■ • ■ । < ।.. । ■ ‘'i''•' i■ i''' ■ r ■'' i' ■ ■ ■ i ■' • ■ i' ■■ ■ i'' ■ ■ i 10 20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 T‘ 5.60 m/ z 5.80 43.10 L ' ' ' 1 1 ' ' ' I ' ' 600 6.20 25.34% Abundance #78238: Acetic acid, 3-[1,3]dioxolan-2-ylpropyl ester 73

5000 5.60 5.80 6.00 6.20 43 m/z 41.10 9.65% 27 55 .1 87 113 174 0 11 ■ । 'i ■ Ip n/z-> 10 20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 Abundance #36138:3-(CYCLOHEX-3'-EN-YL)PROPANOL $$ 2-Cyclohexene-1-p... 73 **/nd/m//mmnmm 5.60 5.80 6.00 6.20 5000 m/z 45.10 9.39%

L 43 27 87 55 01" i1" ’ i " " i' TIN ■ i , I r 113 +p T‘TT i ■ " ' i ■ " ■ r ' " i' " ' i 174 TTTi rn/z--> 10 20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 Abundance #4814: Silane, tetramethyl- 73 5.60 5.80 6.00 6.20 m/z 71.10 6.60%

5000

45 | 53 15 11'''' r TPpmt 0 ' ’ i ■'' I 88 Tuuu—muuw—n"nmmna‘nnu—m—Bm T‘ AI m/z-> 10 20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 5.60 5.80 6.00 6.20

00467.D SCAN508.M Mon Jan 14 10:47:06 2002 Page 3

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