GCMS results for sample AE00740, Jan 29 2002

NYC 9/11 Public Portal Document

Library Search Compound Report

’ Data File : C:\MSDCHEM\1\5973N\02JAN16\00740.D Vial: 8 Acq On : 16 Jan 2002 8:57 pm Operator: Sample : 508scan Inst : Instrumen Mise : January 16, 2002 Multiplr: 1.00 MS Integration Params: LSCINT.P Quant Method : C:\MSDCHEM\1... \SCAN508.M (RTE Integrator) Title : 508 scan method Library : C:\DATABASE\WILEY7N.L ********************************************************************* Peak Number 3 Acetic acid, 3-[1,3]dioxola... Concentration Rank 1

R.T. EstConc Area Relative to ISTD R.T.

5.89 4.71 ug/L 1868470 1,4-Dichlorobenzene-d4 9.71

Hit# Of 5 Tentative ID MW MolForm • CAS# Qual 1 Acetic acid, 3-[1,3]dioxolan-2-y... 174 C8H14O4 000000-00-0 33 2 3-(CYCLOHEX-3 ‘ -EN-YL)PROPANOL $$... 174 C8H14O4 015745-87-6 33 3 N-Ethylformamide $$ N-Formylethy... 73 C3H7NO 000627-45-2 9 4 Silane, tetramethyl- 88 C4H12Si 000075-76-3 9 Abundance Scan 220 (5.885 min): 00740.D (-) " 73.10 100.00% 73

5000 43 5.60 5.80 6.00 6.20 . 87 103 01........................ -- TT m/z 43.10 23.43% m/z-> 10 20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 Abundance #78238: Acetic acid, 3-[1,3]dioxolan-2-ylpropyl ester 73

5000 5.60 5.80 6.00 6.20 43 m/z 45.10 9.01% 27 55 .। 87 113 174 01 i ■ ■ " i ■ ■ • ■ i P1....... । ■ i ■ TTT i ■1 ■ ■ r ’ • • i ■ ■ ‘' i r "' r /z-> 10 20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 Abundance #36138:3-(CYCLOHEX-3'-EN-YL)PROPANOL $$ 2-Cyclohexene-1-p... 73 5.60 5.80 6.00 6.20 5000 m/z 41.10 8.58% 43 27 55 .I 87 113 174 0-biyoninure) ' ‘I.... " T1 ....... . i""r' i1" ' r ■ " i ■ " ' i r”■r Tl/Z-> 10 20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 Abundance #1794: N-Ethylformamide $$ N-Formylethylamine $$ Formamide... 3b 5.60 5.80 6.00 6.20 73 m/z 71.10 6.66%

5000 44 58

15 I 0 l *' " I i " ' ■ 11 '■i" ' ■ i'' ■■i'■ ■ ■ i' ■' • i i1 " ■ i" " r " ' r " ■ i 1" ------- m/z-> 10 20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 5.60 5.80 6.00 6.20

)0740.D SCAN508.M Thu Jan 17 08:17:57 2002 Page 5

NYC-WTC_000051992