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← Document results/DEP Box 28/GCMS X 1/8/02 A 1/10/02
Document / 16 pages

GCMS analysis results for sample AE00328, Jan 18 2002

Machine-extracted title · confidence 100%

Laboratory report documenting gas chromatography-mass spectrometry analysis of environmental sample AE00328 conducted on January 18, 2002.

NYC-WTC_000051206–000051221

Folder label: “GCMS X 1/8/02 A 1/10/02”

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NYC 9/11 Public Portal Document

Library Search Compound Report Data File : C:\MSDCHEM\1\5973N\02JAN10\00327.D Vial: 3 Acq On 10 Jan 2002 2:00 pm Operator: Sample : 508 scan ext 1/8 Inst : Instrumen Mise : January 10, 2002 Multiplr: 1.00 MS Integration Params: LSCINT.P

Quant Method : C:\MSDCHEM\1...\SCAN508.M (RTE Integrator) Title : 508 scan method Library : C:\DATABASE\WILEY7N.L ***************************************** *** * ********* ** ** ** * * * * * * *** Peak Number 5 Acetic acid, 3-[1,3]dioxola... Concentration Rank 1 R.T. EstConc Area Relative to ISTD R.T. 5.89 4.34 ug/L 1402260 1,4-Dichlorobenzene-d4 9.72 Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 Acetic acid, 3-[1,3]dioxolan-2-y... 174 C8H14O4 000000-00-0 33 2 3 -(CYCLOHEX-3'-EN-YL)PROPANOL $$... 174 C8H14O4 015745-87-6 33 3 N-Ethylformamide $$ N-Formylethy... 73 C3H7NO 000627-45-2 9 4 1-Propene-1-thiol 74 C3H6S 000925-89-3 9 Abundance Scan 220 (5.886 min): 00327.0 (-) m/z 73.10 100.00% 73 _ y I I | ITI I 5000 43 5.60 5.80 6.00 6.20 o1........... —ll TTTTTTTTI 55 , 11 ' " i " 87i ■ " ' 103 i " i ■ ■■1 r " ■ i ■ " ■ i m/z 43.10 24.97% m/z-> 10 20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 Abundance #78238: Acetic acid, 3-[1,3Jdioxolan-2-ylpropyl ester 78

5000 5.60 5.80 6.00 6.20 43 m/ z 45.10 9.60% 27 55 , 87 H3 174 01■i■■"i■"■i 1 *ri ‘1, WTTTTFFTFrrr/’ । < ij 111111 in 11 ii TT’Tr’I 111111 TI+T ■ r ■1 ’ i " ■ 'T m/z-> 10 20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 Abundance #36138: 3-(CYCLOHEX-3'-EN-YL)PROPANOL $$ 2-Cyclohexene-1-p... 70 560 5.80 6.00 6.20 5000 m/z 41.10 9.47%

1 43 27 55 87 113 174 01" 1111111" ' r TTTI4 ' r " ' i " ' 'i' +) m/z-> 10 20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 Abundance #1794: N-Ethylformamide $$ N-Formylethylamine $$ Formamide... ■ 1 I 1 1 30 5.60 5.80 6.00 6.20 73 m/z 71.10 6.32% 5000 44 58

15

/z-> 0 ipodoomp lI-por i " " i11" i'11' i1 " ' i " ■' i " " r " ' i " " r " ' i " '11" " i " " i' 10 20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 ' I I ' I ' 1 1 1 I I 1 1 1 1 II I 11 5.60 5.80 6.00 6.20

0327.D SCAN508.M Fri Jan 11- 10:08:17 2002 Page 7

NYC-WTC_000051216

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NYC-WTC_000051216Source: NYC Law Department, mirrored locally

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DEP GCMS data table, Jan-Feb 2002 · Box DEP Box 12

NYC-WTC_000004494

Multi-page laboratory data sheet containing sample analysis results and metadata for DEP GCMS records from January to February 2002.

1 shared non-person entities · 1 shared topics · similarity 0.996

machine-extracted · confidence unavailable · Check page ↗
DEP GCMS data table, Jan-Feb 2002 · Box DEP Box 12

NYC-WTC_000003981

Multi-page laboratory data sheet containing sample analysis results and metadata for DEP GCMS records from January to February 2002.

1 shared non-person entities · 1 shared topics · similarity 0.996

machine-extracted · confidence unavailable · Check page ↗

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